Preliminary results of CoQtz-N: A quartz reference material for terrestrial in situ cosmogenic 10Be and 26Al measurements

被引:33
作者
Binnie, S. A. [1 ]
Dewald, A. [2 ]
Heinze, S. [2 ]
Voronina, E. [1 ]
Hein, A. [3 ]
Wittmann, H. [4 ]
von Blanckenburg, F. [4 ]
Hetzel, R. [5 ]
Christl, M. [6 ]
Schaller, M. [7 ]
Leanni, L. [8 ]
Hippe, K. [6 ]
Vockenhuber, C. [6 ]
Ivy-Ochs, S. [6 ]
Maden, C. [9 ]
Fulop, R-H [10 ,11 ]
Fink, D. [11 ]
Wilcken, K. M. [11 ]
Fujioka, T. [11 ]
Fabel, D. [12 ]
Freeman, S. P. H. T. [12 ]
Xu, S. [12 ]
Fifield, L. K. [13 ]
Akcar, N. [14 ]
Spiegel, C. [15 ]
Dunai, T. J. [1 ]
Aumaitre, G. [8 ]
Bourles, D. L.
Keddadouche, K.
机构
[1] Univ Cologne, Inst Geol & Mineral, Zulpicher Str 49b, D-50674 Cologne, Germany
[2] Univ Cologne, Inst Kernphys, D-50937 Cologne, Germany
[3] Univ Edinburgh, Sch GeoSci, Drummond St, Edinburgh EH8 9XP, Midlothian, Scotland
[4] Helmholtz Ctr Potsdam, GFZ German Res Ctr Geosci, D-14473 Potsdam, Germany
[5] Westfalische Wilhelms Univ Munster, Inst Geol & Palaontol, Corrensstr 24, D-48149 Munster, Germany
[6] Swiss Fed Inst Technol, Lab Ion Beam Phys, CH-8093 Zurich, Switzerland
[7] Univ Tubingen, Dept Geosci, Wilhelmstr 56, D-72074 Tubingen, Germany
[8] Aix Marseille Univ, Coll France, CNRS, IRD,UM CEREGE 34, Technopole Environm Arbois Mediterranee,BP80, F-13545 Aix En Provence, France
[9] Swiss Fed Inst Technol, Inst Geochem & Petrol, CH-8092 Zurich, Switzerland
[10] Univ Wollongong, Sch Earth & Environm Sci, Wollongong, NSW 2522, Australia
[11] ANSTO, Lucas Heights, NSW 2234, Australia
[12] SUERC, East Kilbride G75 0QF, Scotland
[13] Australian Natl Univ, Res Sch Phys Sci & Engn, Dept Nucl Phys, Canberra, ACT 0200, Australia
[14] Univ Bern, Inst Geol Sci, Baltzerstr 1-3, Bern, Switzerland
[15] Univ Bremen, Geowissensch FB5, Postfach 330 440, D-28344 Bremen, Germany
关键词
Al-26; Be-10; CoQtz-N; Cosmogenic nuclides; Reference material; ACCELERATOR MASS-SPECTROMETRY; EXERCISE;
D O I
10.1016/j.nimb.2019.04.073
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
There is growing interest in geochronological applications of terrestrial in situ-produced cosmogenic nuclides, with the most commonly measured being Be-10 and Al-26 in quartz. To extract and then separate these radio-nuclides from quartz and prepare them in the oxide form suitable for accelerator mass spectrometry (AMS) requires extensive and careful laboratory processing. Here we discuss the suitability of a crushed, sieved and etched, sub-aerially exposed vein quartz specimen (CoQtz-N) to act as a reference material for chemical laboratory preparation and AMS measurements. Splits of CoQtz-N were distributed to eleven target preparation laboratories. The CoQtz-N Be-10 targets were then measured at seven different AMS facilities and five of the preparation laboratories had their Al-26 targets measured at four different AMS facilities. We show that CoQtz-N splits are sufficiently homogeneous with regard to nuclide concentrations, that it has been cleaned of any atmospheric derived (i.e. meteoric) Be-10 and that it has low concentrations of the major elements that can interfere with Be and Al extraction chemistry and AMS measurements. We derive preliminary concentrations for Be-10 and Al-26 in CoQtz-N as 2.53 +/- 0.09 x 10(6) at/g and 15.6 +/- 1.6 x 10(6) at/g, respectively, at the 95% confidence limit.
引用
收藏
页码:203 / 212
页数:10
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