Synthesis and characterization of porous CaCO3 micro/nano-particles

被引：43

作者：

Achour, A. ^{[1
,2
]}

Arman, A. ^{[3
]}

Islam, M. ^{[4
]}

Zavarian, A. A. ^{[3
]}

Al-Zubaidi, A. Basim ^{[5
]}

Szade, J. ^{[2
]}

机构：

[1] INRS, 1650 Blvd Lionel Boulet, Varennes, PQ J3X 1P7, Canada

[2] Univ Silesia, August Chelkowski Inst Phys, Dept Solid State Phys, Uniwersytecka 4, PL-40007 Katowice, Poland

[3] ACECR, Vacuum Technol Grp, Sharif Branch, Tehran, Iran

[4] King Saud Univ, CEREM, POB 800, Riyadh 11421, Saudi Arabia

[5] Univ Technol Baghdad, Dept Mat Engn, POB 35095, Baghdad, Iraq

来源：

EUROPEAN PHYSICAL JOURNAL PLUS | 2017年 / 132卷 / 06期

关键词：

CALCIUM-CARBONATE; HYALURONIC-ACID; ELECTRICAL-PROPERTIES; RAMAN; VATERITE;

D O I：

10.1140/epjp/i2017-11531-8

中图分类号：

O4 [物理学];

学科分类号：

0702 ;

摘要：

Porous CaCO3 particles, both micro and nano sized, were synthesized in a mixture of Ca(OH)(2), hyaluronic acid (HA), glycine, NaOH and NaCl solution with supercritical carbon dioxide. The particles were characterized using X-Ray Diffraction (XRD), Fourier Transform Infrared (FTIR) spectroscope, Raman spectroscope (RS), X-ray photoelectron spectroscope (XPS) and scanning electron microscope techniques. All these techniques showed that the particles crystallize into only one CaCO3 structure, namely the vaterite phase. In addition, FTIR, RS and XPS indicated the presence of residual reactive species i.e. glycine, NaCl, and HA. The XRD results confirmed the presence of NaCl and gamma-glycine, which is a crystalline material. Moreover, the HA seems to be mostly embedded in the bulk of the micro-particles. Such materials are promising for biomedical applications such as drug delivery.

引用

页数：9

共 50 条

[1] Synthesis and characterization of porous CaCO3 micro/nano-particles
A. Achour
A. Arman
M. Islam
A. A. Zavarian
A. Basim Al-Zubaidi
J. Szade
The European Physical Journal Plus, 132
[2] SYNTHESIS OF MICRO-COMPOSITE BEADS WITH MAGNETIC NANO-PARTICLES EMBEDDED IN POROUS CaCO3 MATRIX
Vesel, Alenka
Kosak, Aljoska
Halozan, David
Elersic, Kristina
MATERIALI IN TEHNOLOGIJE, 2012, 46 (01): : 57 - 61
[3] Synthesis of nano-particles of CaCO3 in a novel reactor
Chen, J
Wang, Y
Jia, Z
Zheng, C
2ND INTERNATIONAL CONFERENCE ON PROCESS INTENSIFICATION IN PRACTICE: APPLICATIONS AND OPPORTUNITIES, 1997, (28): : 157 - 164
[4] Influence of CaCO3 micro- and nano-particles on the structure and properties of Nylon-66
Ghadami, Aboutaleb
Ghadam, Jadval
BULGARIAN CHEMICAL COMMUNICATIONS, 2015, 47 : 19 - 34
[5] Preparing of CaCO3 Nano-particles by Mechano-chemical Method
Sargheini, J.
Ataie, A.
Salili, S. M.
Johari, M.
Hadad, M.
MATERIALS AND MANUFACTURING TECHNOLOGIES XIV, 2012, 445 : 833 - +
[6] Synthesis and Characterization of Porous CaCO3 Vaterite Particles by Simple Solution Method
Febrida, Renny
Cahyanto, Arief
Herda, Ellyza
Muthukanan, Vanitha
Djustiana, Nina
Faizal, Ferry
Panatarani, Camellia
Joni, I. Made
MATERIALS, 2021, 14 (16)
[7] Synthesis of CaCO3 nano- and micro-particles by dry ice carbonation
Donnelly, F. C.
Purcell-Milton, F.
Framont, V.
Cleary, O.
Dunne, P. W.
Gun'ko, Y. K.
CHEMICAL COMMUNICATIONS, 2017, 53 (49) : 6657 - 6660
[8] Study on preparation of water-soluble CaCO3 nano-particles and their tribological properties
Yu, Guoxian
Sun, Mobin
Zhou, Xiaolong
Li, Chenglie
Shiyou Xuebao, Shiyou Jiagong/Acta Petrolei Sinica (Petroleum Processing Section), 2012, 28 (01): : 137 - 142
[9] Synthesis and characterization of silver nano-particles
Zhang, Xiaomin
Zhang, Zhenzhong
Zhao, Fangxia
Zhou, Hao
Qiu, Tai
Zhenkong Kexue yu Jishu Xuebao/Journal of Vacuum Science and Technology, 2013, 33 (10): : 1037 - 1041
[10] Synthesis and Characterization of Nano-Sized CaCO3 in Purified Diet
Mulyaningsih, N. N.
Tresnasari, D. R.
Ramahwati, M. R.
Juwono, A. L.
Soejoko, D. S.
Astuti, D. A.
INTERNATIONAL SYMPOSIUM ON CURRENT PROGRESS IN MATHEMATICS AND SCIENCES 2016 (ISCPMS 2016), 2017, 1862

← 1 2 3 4 5 →