Improved critical current density in ex situ processed MgB2 tapes by the size reduction of grains and crystallites by high-energy ball milling

We have fabricated Fe-sheathed MgB2 tapes through an ex situ process in a powder-in-tube (PIT) technique using powders ball milled under various conditions. Although the ex situ processed wires and tapes using the high-energy ball milled MgB2 powders have been studied and the decrease of grain and crystallite sizes of MgB2 and the critical current density (J(c))improvement of those conductors were reported so far, the use of filling powders milled at a higher rotation speed than previously reported further decreases the crystallite size and improves the J(c) properties. The improved J(c) values at 4.2 K and 10 T were nearly twice as large as those previously reported. Those milled powders and hence as-rolled tapes easily receive contamination in air. Thus, the transport J(c)operties are easily deteriorated and scattered unless the samples are handled with care. The optimized heat treatment temperature (T-opt) of those tape samples at which best performance in the Jr property is obtained decreases by more than 100 degrees C, compared with that of tapes using the as -received MgB2 powder.(C) 2017 Elsevier Ltd. All rights reserved.