Synthesis and characterization of flower-like MoS2 microspheres by a facile hydrothermal route

被引：49
作者：
Ma, Lin [1 ,2 ]
Xu, Li-Mei [1 ]
Xu, Xu-Yao [1 ]
Luo, Yang-Li [1 ]
Chen, Wei-Xiang [2 ]
机构：
[1] Zhanjiang Normal Univ, Chem Sci & Technol Sch, Zhanjiang 524048, Peoples R China
[2] Zhejiang Univ, Dept Chem, Hangzhou 310027, Zhejiang, Peoples R China
来源：
MATERIALS LETTERS | 2009年 / 63卷 / 23期
关键词：
MoS2; Microspheres; Crystal growth; Nanomaterials; ELECTROCHEMICAL HYDROGEN STORAGE; CHEMICAL-VAPOR-DEPOSITION; SONOCHEMICAL PREPARATION; SOLID-STATE; ONE-STEP; NANOTUBES; WS2; NANOSTRUCTURES; NANOPARTICLES; NANOFLOWERS;
D O I：
10.1016/j.matlet.2009.06.039
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Flower-like MoS2 microspheres with high purity were successfully synthesized via a facile hydrothermal route by adding sodium silicate as an additive. The products were characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM) and scanning electron microscopy (SEM). XRD patterns showed that the MoS2 microspheres had good crystallinity with well-stacked layered structure. TEM and SEM images showed that the MoS2 microspheres had uniform sizes with mean diameter about 480 nm and were constructed with MoS2 sheets with thickness of several nanometers. it was found that the possible precursor H4SiMo12O40 obtained by sodium silicate reacting with sodium molybdate played a crucial role in the formation of the flower-like MoS2 microspheres in our experiment. A possible formation mechanism of MoS2 microspheres was preliminarily presented. (C) 2009 Elsevier B.V. All rights reserved.
引用
收藏
页码：2022 / 2024
页数：3
相关论文
共 50 条
  • [31] Hydrothermal synthesis and characterization of novel flowerlike MoS2 hollow microspheres
    Tang, Guogang
    Wang, Yijiang
    Chen, Wei
    Tang, Hua
    Li, Changsheng
    MATERIALS LETTERS, 2013, 100 : 15 - 18
  • [32] A facile hydrothermal route to flower-like single crystalline EuPO4 • H2O
    Chen, Yang
    Wei, Xian-Wen
    Wu, Kong-Lin
    Liu, Xiao-Wang
    MATERIALS LETTERS, 2012, 89 : 108 - 110
  • [33] Controllable growth of MoS2/C flower-like microspheres with enhanced electrochemical performance for lithium ion batteries
    Xiong, Q. Q.
    Ji, Z. G.
    JOURNAL OF ALLOYS AND COMPOUNDS, 2016, 673 : 215 - 219
  • [34] Hydrothermal synthesis and controlled growth of hierarchical 3D flower-like MoS2 nanospheres assisted with CTAB and their NO2 gas sensing properties
    Zhang, Yajie
    Zeng, Wen
    Li, Yanqiong
    APPLIED SURFACE SCIENCE, 2018, 455 : 276 - 282
  • [35] Hydrothermal synthesis and characterization of NiS flower-like architectures
    Zhou, Hai
    Lv, Baoliang
    Wu, Dong
    Sun, Yuhan
    PARTICUOLOGY, 2012, 10 (06) : 783 - 788
  • [36] Hydrothermal synthesis and characterization of MoS2 nanorods
    Lin, Hongtao
    Chen, Xiaoya
    Li, Hongling
    Yang, Min
    Qi, Yanxing
    MATERIALS LETTERS, 2010, 64 (15) : 1748 - 1750
  • [37] Synthesis and characterization of flowerlike MoS2 nanostructures through CTAB-assisted hydrothermal process
    Tang, Guogang
    Sun, Jianrong
    Wei, Chen
    Wu, Kongqiang
    Ji, Xiaorui
    Liu, Shuaishuai
    Tang, Hua
    Li, Changsheng
    MATERIALS LETTERS, 2012, 86 : 9 - 12
  • [38] Facile Synthesis of Hollow MoS2 Microspheres/Amorphous Carbon Composites and Their Lithium Storage Properties
    Qiu, Wenda
    Xia, Jian
    He, Shenxian
    Xu, Hongji
    Zhong, Haimin
    Chen, Liuping
    ELECTROCHIMICA ACTA, 2014, 117 : 145 - 152
  • [39] Synthesis and characterization of tubular CuS with flower-like wall from a low temperature hydrothermal route
    Chen, Lifei
    Yu, Wei
    Li, Yang
    POWDER TECHNOLOGY, 2009, 191 (1-2) : 52 - 54
  • [40] Synthesis and Characterization of Flower-Like ZnO Microspheres Assembled by Nanosheets
    Lei, Ying
    Wu, Xiang
    Qu, Fengyu
    ADVANCED SCIENCE LETTERS, 2011, 4 (11-12) : 3608 - 3612
12345