5-Methoxymethyl-4-phenoxy-1H-pyrazol-3-ol

被引:13
作者
Shahani, Tara [1 ]
Fun, Hoong-Kun [1 ]
Ragavan, R. Venkat [2 ]
Vijayakumar, V. [2 ]
Sarveswari, S. [2 ]
机构
[1] Univ Sains Malaysia, Sch Phys, Xray Crystallog Unit, USM, George Town 11800, Malaysia
[2] VIT Univ, Div Organ Chem, Sch Adv Sci, Vellore 632014, Tamil Nadu, India
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷
关键词
X-RAY;
D O I
10.1107/S1600536809050302
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C11H12N2O3, the pyrazole ring system is essentially planar [maximum deviation = 0.002 (2) angstrom] and forms a dihedral angle of 66.93 (9)degrees with the benzene ring. In the crystal packing, pairs of intermolecular N-H center dot center dot center dot O and O-H center dot center dot center dot N hydrogen bonds connect neighbouring molecules into dimers, generating R-2(2)(10) and R-2(2)(8) ring motifs, respectively. The crystal structure is further stabilized by C-H center dot center dot center dot interactions.
引用
收藏
页码:O3249 / U1961
页数:11
相关论文
共 50 条
  • [41] Ethyl 5-cyano-8-nitro-2,3,4,4a,5,6-hexahydro-1H-pyrido[1,2-a]quinoline-5-carboxylate
    Yapo, Yapi Marcellin
    Konan, Kouakou Michel
    Adjou, Ane
    Timotou, Adeyole
    Tenon, Jules A.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1735 - U849
  • [42] Ethyl 1-tert-butyl-5-phenyl-1H-pyrazole-4-carboxylate
    Fun, Hoong-Kun
    Quah, Ching Kheng
    Chandrakantha, B.
    Isloor, Arun M.
    Shetty, Prakash
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O2228 - U1593
  • [43] Base Stabilized σ-Borane Complex of Group 5 Metals: Synthesis and Structure of [(η5-C5Me5)Ta(H3BNC5H4) (C5H4NS)(η2-S2)]
    Haridas, Anagha
    Saha, Suvam
    Bedajna, Shantabh
    Ghosh, Sundargopal
    EUROPEAN JOURNAL OF INORGANIC CHEMISTRY, 2023, 26 (27)
  • [44] 1-Benzyl-5-methoxy-2',3-dimethyl-4,6-dioxa-2-azaspiro[bicyclo[3.2.0]hept-2-ene-7,4'-isoquinoline]-1',3'(2'H,4'H)-dione
    Fun, Hoong-Kun
    Quah, Ching Kheng
    Huang, Chengmei
    Yu, Haitao
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1311 - U1910
  • [45] Organotin(IV) polypyrazolylborates .9. Tetrakis(4-methyl-1H-pyrazol-1-yl)borates. Characterisation, Mossbauer study and X-ray crystal structure of Cl3Sn(mu-4-MePz)(3)B(4-MePz)
    Lobbia, GG
    Cecchi, P
    Santini, C
    Calogero, S
    Valle, G
    Wagner, FE
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1996, 513 (1-2) : 139 - 146
  • [46] 4-(4-(( 5-Amino-1,3,4-thiadiazol-2-yl)methoxy) phenyl)-1-(( 5-amino-1,3,4-thiadiazol-2-yl)methyl)-3-benzyl-1H-1,2,4-triazol-5( H)-one: Synthesis, Characterization and Computational Studies
    Unluer, Dilek
    Unver, Yasemin
    Dugdu, Esra
    Akcay, Hakki Turker
    Sancak, Kemal
    LETTERS IN ORGANIC CHEMISTRY, 2016, 13 (08) : 604 - 617
  • [47] (1Z,2E)-1-(3,5-dimethyl-1H-pyrazol-1-yl)ethane-1,2-dione dioxime
    Sarikavakli, Nursabah
    Sahin, Ertan
    Hokelek, Tuncer
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O3601 - U4350
  • [48] Structure and magnetism of electrospun porous high-entropy (Cr1/5Mn1/5Fe1/5Co1/5Ni1/5)3O4, (Cr1/5Mn1/5Fe1/5Co1/5Zn1/5)3O4 and (Cr1/5Mn1/5Fe1/5Ni1/5Zn1/5)3O4 spinel oxide nanofibers
    Ponti, Alessandro
    Triolo, Claudia
    Petrovicova, Beatrix
    Ferretti, Anna M.
    Pagot, Gioele
    Xu, Wenlei
    Di Noto, Vito
    Pinna, Nicola
    Santangelo, Saveria
    PHYSICAL CHEMISTRY CHEMICAL PHYSICS, 2023, 25 (03) : 2212 - 2226
  • [49] Organotin(IV) polypyrazolylborates .12. Hydridotris(4-bromo-1H-pyrazol-1-yl)borates: Characterization, Mossbauer study and X-ray crystal structure of MeCl(2)Sn(4-BrPz)(3)BH
    Calogero, S
    Valle, G
    Lobbia, GG
    Santini, C
    Cecchi, P
    Stievano, L
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1996, 526 (02) : 269 - 277
  • [50] Crystal structure, Hirshfeld surface and frontier molecular orbital analysis of 9-(3-bromo-4-hydroxy5-methoxypheny1)-3,3,6,6-tetramethy1-3,4,5,6,7,9- hexahydro-1H-xanthene-1,8(2H)-dione
    Babu, N. Suresh
    Sughanya, V
    Praveenkumar, D.
    Sundararajan, M. L.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2021, 77 : 1170 - +