5-Methoxymethyl-4-phenoxy-1H-pyrazol-3-ol

被引:13
|
作者
Shahani, Tara [1 ]
Fun, Hoong-Kun [1 ]
Ragavan, R. Venkat [2 ]
Vijayakumar, V. [2 ]
Sarveswari, S. [2 ]
机构
[1] Univ Sains Malaysia, Sch Phys, Xray Crystallog Unit, USM, George Town 11800, Malaysia
[2] VIT Univ, Div Organ Chem, Sch Adv Sci, Vellore 632014, Tamil Nadu, India
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷
关键词
X-RAY;
D O I
10.1107/S1600536809050302
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C11H12N2O3, the pyrazole ring system is essentially planar [maximum deviation = 0.002 (2) angstrom] and forms a dihedral angle of 66.93 (9)degrees with the benzene ring. In the crystal packing, pairs of intermolecular N-H center dot center dot center dot O and O-H center dot center dot center dot N hydrogen bonds connect neighbouring molecules into dimers, generating R-2(2)(10) and R-2(2)(8) ring motifs, respectively. The crystal structure is further stabilized by C-H center dot center dot center dot interactions.
引用
收藏
页码:O3249 / U1961
页数:11
相关论文
共 50 条
  • [21] 3,5-Diphenyl-1-(quinolin-2-yl)-4,5-dihydro-1H-pyrazol-5-ol
    Bin Najib, Muhd. Hidayat
    Tan, Ai Ling
    Young, David J.
    Ng, Seik Weng
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : 02310 - +
  • [22] 4-[(3-Hydroxy-5-phenyl-1H-pyrazol-4-yl)-methyl]-5-phenyl-1H-pyrazol-3(2H)-one
    Baryala, Yamna
    Zerzouf, Abdelfettah
    Essassi, El Mokhtar
    Reuter, Hans
    Eickmeier, Henning
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O2554 - O2556
  • [23] 1-(4-chlorophenyl)-4-(2-furoyl)-3-(2-furyl)-1H-pyrazol-5-ol
    Li, Jin-Zhou
    Zhang, Heng-Qiang
    Li, Hong-Xin
    Che, Pi-Zhi
    Wang, Tian-Chi
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : o1289 - o1290
  • [24] Synthesis of 4,4 '-(Cyclohexane-1,1-diyl)bis(1-methyl-1H-pyrazol-5-ol)
    Eller, Gernot A.
    Holzer, Wolfgang
    MOLBANK, 2008, (02)
  • [25] Synthesis of 4,5-dihydropyrazolyl-2H-indenediones by aldol condensation of ninhydrin with 1H-pyrazol-5-ol
    Soleimani, Ebrahim
    Hariri, Mina
    Rostamzadeh, Arman
    Ghorbani, Somayeh
    JOURNAL OF CHEMICAL RESEARCH, 2016, (11) : 664 - 666
  • [26] Synthesis and antibacterial activity of 4,4'-(aryl or alkyl methylene)-bis(1H-pyrazol-5-ol) derivatives
    Bhavanarushi, S.
    Kanakaiah, V.
    Bharath, Gandu
    Gangagnirao, A.
    Rani, J. Vatsala
    MEDICINAL CHEMISTRY RESEARCH, 2014, 23 (01) : 158 - 167
  • [27] Synthesis and antibacterial activity of 4,4′-(aryl or alkyl methylene)-bis(1H-pyrazol-5-ol) derivatives
    S. Bhavanarushi
    V. Kanakaiah
    Gandu Bharath
    A. Gangagnirao
    J. Vatsala Rani
    Medicinal Chemistry Research, 2014, 23 : 158 - 167
  • [28] 3-Methyl-5-phenoxy-1-phenyl-1H-pyrazole-4-carbaldehyde
    Shahani, Tara
    Fun, Hoong-Kun
    Shetty, Shobhitha
    Kalluraya, Balakrishna
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2646 - +
  • [29] The synthesis of 4,4'-arylmethylene-bis(3-(trifluoromethyl)-1-phenyl-1H-pyrazol-5-ol) in aqueous media without catalyst
    Yao, Chang-Sheng
    Yu, Chen-Xia
    Tu, Shu-Jiang
    Shi, Da-Qing
    Wang, Xiang-Shan
    Zhu, You-Quan
    Yang, Hua-Zheng
    JOURNAL OF FLUORINE CHEMISTRY, 2007, 128 (02) : 105 - 109
  • [30] 3-ethoxycarbonyl-1-phenyl-1H-pyrazol-5-yl4-chlorobenzoate
    Zheng, PW
    Fan, ML
    Duan, XM
    Li, JS
    Huang, PM
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O311 - O312