5-Methoxymethyl-4-phenoxy-1H-pyrazol-3-ol

被引：13

作者：

Shahani, Tara ^{[1
]}

Fun, Hoong-Kun ^{[1
]}

Ragavan, R. Venkat ^{[2
]}

Vijayakumar, V. ^{[2
]}

Sarveswari, S. ^{[2
]}

机构：

[1] Univ Sains Malaysia, Sch Phys, Xray Crystallog Unit, USM, George Town 11800, Malaysia

[2] VIT Univ, Div Organ Chem, Sch Adv Sci, Vellore 632014, Tamil Nadu, India

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷

关键词：

X-RAY;

D O I：

10.1107/S1600536809050302

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C11H12N2O3, the pyrazole ring system is essentially planar [maximum deviation = 0.002 (2) angstrom] and forms a dihedral angle of 66.93 (9)degrees with the benzene ring. In the crystal packing, pairs of intermolecular N-H center dot center dot center dot O and O-H center dot center dot center dot N hydrogen bonds connect neighbouring molecules into dimers, generating R-2(2)(10) and R-2(2)(8) ring motifs, respectively. The crystal structure is further stabilized by C-H center dot center dot center dot interactions.

引用

页码：O3249 / U1961

页数：11

共 50 条

[11] Synthesis of 4,4′-(arylmethylene)bis(3-methyl-1H-pyrazol-5-ol) derivatives in water
Soleimani, Ebrahim
Ghorbani, Somayeh
Taran, Mojtaba
Sarvary, Afshin
COMPTES RENDUS CHIMIE, 2012, 15 (11-12) : 955 - 961
[12] (E)-2-[(3-Methyl-5-phenoxy-1-phenyl-1H-pyrazol-4-yl) methylidene]hydrazinecarbothioamide
Fun, Hoong-Kun
Quah, Ching Kheng
Shetty, Shobhitha
Kalluraya, Balakrishna
Nitinchandra
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O2146 - +
[13] A unique tautomer of 1-n-hexyl-3-phenyl-1H-pyrazol-5-ol
Belmar, Julio
Jimenez, Claudio
Ruiz-Perez, C.
Delgado, F. S.
Baggio, Ricardo
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 2006, 62 : O599 - O601
[14] 3-Phenyl-1-(2-pyridyl)-1H-pyrazol-5-ol
McFerrin, Cheri A.
Hammer, Robert P.
Fronczek, Frank R.
Watkins, Steven F.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O2518 - O2519
[15] 4-{(2,4-Dichlorophenyl)[5-hydroxy-1-phenyl-3-(trifluoromethyl)-1H-pyrazol-4yl]methyl}-1-phenyl-3(trifluoromethyl)-1H-pyrazol-5-ol monohydrate
Yao, CS
Yu, CX
Tu, SJ
Wang, XS
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O771 - O773
[16] Chemistry of 4,4-(arylmethylene)-bis(3-methyl-1-phenyl-1H-pyrazol-5-ol)s
Gouda, Moustafa A.
JOURNAL OF HETEROCYCLIC CHEMISTRY, 2016, 53 (02) : 356 - 376
[17] 4,4 '-[(2-Chlorophenyl) methylene] bis[1-phenyl-3-(trifluoromethyl)-1H-pyrazol-5-ol]
Guo, Changbin
Holzer, Wolfgang
MOLBANK, 2009, (03)
[18] Efficient preparation of potassium arylmethylene-4-(1H-pyrazol-5-ol)-4′-(1H-pyrazol-5-olate) derivatives via a four-component reaction
Wang, Ting
Yu, Yang
Qing, Xushun
Dai, Chenlu
Wang, Cunde
JOURNAL OF CHEMICAL RESEARCH, 2018, (06) : 313 - 316
[19] Design, synthesis, antimicrobial evaluations and in silico studies of novel pyrazol-5(4H)-one and 1H-pyrazol-5-ol derivatives
Pham, Em Canh
Tuong Vi Le Thi
Phan, Long Tieu
Nguyen, Huong-Giang T.
Le, Khanh N. B.
Tuyen Ngoc Truong
ARABIAN JOURNAL OF CHEMISTRY, 2022, 15 (03)
[20] 5-methyl-2-phenyl-2H-pyrazol-3-ol
Wang, Qiang
Zhang, Yi
Wang, Rong
Yang, Yi-Lin
Zhi, Feng
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1924 - U3769

← 1 2 3 4 5 →