A novel and efficient synthesis of unsymmetrical disulfides

被引:46
作者
Antoniow, Sylwia [1 ]
Witt, Dariusz [1 ]
机构
[1] Gdansk Univ Technol, Fac Chem, Dept Organ Chem, PL-80952 Gdansk, Poland
来源
SYNTHESIS-STUTTGART | 2007年 / 03期
关键词
unsymmetrical disulfides; alkanethiols; L-cysteine; thiophenol;
D O I
10.1055/s-2007-965873
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
Unsymmetrical disulfides have been prepared from the corresponding thiols and bis-(5,5-dimethyl-2-thiono-1,3,2-dioxa-phosphorinanyl)disulfide under mild conditions with good to excellent yields. The method can be applied to thiols bearing neutral, aromatic, basic or acidic functionalities with variable length of carbon chain.
引用
收藏
页码:363 / 366
页数:4
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