Powder X-ray data for adenosine C10H13N5O4

被引：3
作者：
Caminiti, R
Ortaggi, G
Mazzei, RA
Ballirano, P
Rizzi, R
机构：
[1] Univ Rome La Sapienza, Dipartimento Chim, Ist Nazl Fis Mat, I-00185 Rome, Italy
[2] Univ Rome La Sapienza, Dipartimento Sci Terra, I-00185 Rome, Italy
[3] TRRE snc, I-40138 Bologna, Italy
来源：
POWDER DIFFRACTION | 2000年 / 15卷 / 02期
关键词：
adenosine; C10H13N5O4; Rietveld refinement; powder diffraction;
D O I：
10.1017/S0885715600010940
中图分类号：
TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
New powder X-ray diffraction data of adenosine C10H13N5O4 were reported: cell parameters are a=4.8386(4) Angstrom, b= 10.2919(4) Angstrom, c= 1 1.8555(4) Angstrom, beta= 99.298(5)degrees volume 582.63(4)Angstrom for the monoclinic space group P2(1). The strongest lines are: 7.723 (100), 5.085 (50), 5.851 (45), 4.710 (11), 3.881 (10), 3.899 (9), 3.292 (9), and 3.261 (9). Reported intensities are validated by Rietveld analysis. The data consist of measured positions and intensities and cover an angular range up to 75 degrees 2 theta and are significantly better than PDF 35-1977. Experimental, calculated, and difference patterns are also reported. (C) 2000 International Centre for Diffraction Data. [S0885-7156(00)00801-0].
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收藏
页码：112 / 115
页数：4
相关论文
共 16 条
[1]   X-ray powder diffraction structure reinvestigation of the α and β forms of cobalt phthalocyanine and kinetics of the α→β phase transition [J].
Ballirano, P ;
Caminiti, R ;
Ercolani, C ;
Maras, A ;
Orrù, MA .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1998, 120 (49) :12798-12807
[2]   Single crystal structure determination of cetylpyridiniumammonium bromide and Rietveld structure determination of cetylquinuclidinium bromide [J].
Ballirano, P ;
Caminiti, R ;
Sadun, C ;
Coiro, VM ;
Mancini, G ;
Maras, A .
ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 1998, 213 (02) :123-129
[3]  
Bunge H. J., 1982, Texture analysis in materials science: mathematical methods
[4]   Powder X-ray data for melatonin C13H16N2O2 [J].
Caminiti, R ;
Ortaggi, G ;
Mazzei, RA ;
Ballirano, P ;
Rizzi, R .
POWDER DIFFRACTION, 2000, 15 (02) :108-111
[5]  
COSTA U, 2000, IN PRESS POWDER DIFF
[6]   A SIMPLIFIED CRITERION FOR RELIABILITY OF A POWDER PATTERN INDEXING [J].
DEWOLFF, PM .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1968, 1 :108-+
[7]   A CORRECTION FOR POWDER DIFFRACTION PEAK ASYMMETRY DUE TO AXIAL DIVERGENCE [J].
FINGER, LW ;
COX, DE ;
JEPHCOAT, AP .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1994, 27 :892-900
[8]  
GARVEY RG, 1986, POWDER DIFFR, V1, P89
[9]   HYDROGEN-BONDING IN NUCLEOSIDES AND NUCLEOTIDES [J].
JEFFREY, GA ;
MALUSZYNSKA, H ;
MITRA, J .
INTERNATIONAL JOURNAL OF BIOLOGICAL MACROMOLECULES, 1985, 7 (06) :336-348
[10]   CRYSTAL-STRUCTURE OF ADENOSINE [J].
LAI, TF ;
MARSH, RE .
ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL CRYSTALLOGRAPHY AND CRYSTAL CHEMISTRY, 1972, B 28 (JUL15) :1982-&
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