Highly sensitive detection of sodium in aqueous solutions using laser-induced breakdown spectroscopy with liquid sheet jets

被引：27
作者：
Nakanishi, Ryuzo [1 ,2 ]
Ohba, Hironori [1 ,2 ]
Saeki, Morihisa [1 ,2 ]
Wakaida, Ikuo [2 ]
Tanabe-Yamagishi, Rie [3 ,4 ]
Ito, Yoshiro [3 ]
机构：
[1] Natl Inst Quantum & Radiol Sci & Thchnol, Quantum Beam Sci Res Directorate, Tokai, Ibaraki 3191106, Japan
[2] Japan Atom Energy Agcy, Collaborat Labs Adv Decommissioning Sci, Tokai, Ibaraki 3191195, Japan
[3] Nagaoka Univ Technol, Dept Mech Engn, Nagaoka, Niigata 9402188, Japan
[4] Fukuoka Inst Technol, Dept Intelligent Mech Engn, Higashi Ku, Fukuoka 8110295, Japan
来源：
OPTICS EXPRESS | 2021年 / 29卷 / 04期
基金：
日本学术振兴会;
关键词：
SPECTROCHEMICAL ANALYSIS; QUANTITATIVE-ANALYSIS; ELEMENTAL ANALYSIS; METAL-IONS; WATER; LIBS; IRON;
D O I：
10.1364/OE.415308
中图分类号：
O43 [光学];
学科分类号：
070207 ; 0803 ;
摘要：
Laser-induced breakdown spectroscopy (LIBS) combined with liquid jets was applied to the detection of trace sodium (Na) in aqueous solutions. The sensitivities of two types of liquid jets were compared: a liquid cylindrical jet with a diameter of 500 mu m and a liquid sheet jet with a thickness of 20 mu m. Compared with the cylindrical jet, the liquid sheet jet effectively reduced the splash from the laser-irradiated surface and produced long-lived luminous plasma. The limit of detection (LOD) of Na was determined to be 0.57 mu g/L for the sheet jet and 10.5 mu g/L for the cylindrical jet. The LOD obtained for the sheet jet was comparable to those obtained for commercially available inductively coupled plasma emission spectrometers. (C) 2021 Optical Society of America under the terms of the OSA Open Access Publishing Agreement
引用
收藏
页码：5205 / 5212
页数：8
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