Spark plasma sintering of LaB6-(Ti, Zr)B2 composites

被引:7
作者
Wang, X. [1 ]
Zhang, J. X. [1 ]
Yang, X. Y. [1 ]
Hu, K. [1 ]
Zhang, J. W. [1 ]
机构
[1] Hefei Univ Technol, Sch Mat Sci & Engn, Hefei 230009, Peoples R China
基金
中国国家自然科学基金;
关键词
LaB6-(Ti; Zr)B-2; composite; spark plasma sintering; microstructure; mechanical property; MECHANICAL-PROPERTIES; INDENTATION FRACTURE; SYSTEM;
D O I
10.1080/17436753.2016.1264139
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The LaB6-(Ti-,Ti- Zr)B-2 composite was fabricated from LaB6, TiB2 and ZrB2 powders by spark plasma sintering (SPS) at 1600-1900 degrees C holding for 5min under 40MPa. The densification behaviour, microstructure, mechanical properties were investigated. The complete solid solution phase of (Ti, Zr)B-2 was identified. The morphologies of LaB6 and (Ti, Zr)B-2 grains were equiaxed and elongated, respectively. The highest relative density of 98.43% and Vickers hardness of 19.56GPa were obtained at 1900 degrees C. The fracture toughness of 4.43MPam(1/2) was obtained at 1800 degrees C.
引用
收藏
页码:132 / 137
页数:6
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