Synthesis and structure of tetraphenylantimony N,N-diethyldithiocarbamate

被引:2
作者
Sharutin, VV [1 ]
Sharutina, OK [1 ]
Platonova, TP [1 ]
Pakusina, AP [1 ]
Krivolapov, DB [1 ]
Gubaidullin, AT [1 ]
Litvinov, IA [1 ]
机构
[1] Blagoveshchensk State Pedag Univ, Blagoveshchensk, Russia
关键词
Sodium; Chloride; Bond Length; Diffraction Data; Diethyldithiocarbamate;
D O I
10.1023/A:1021613526421
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Tetraphenylantimony chloride was reacted with sodium N,N-diethyldithiocarbamate in water to obtain tetraphenylantimony N,N-diethyldithiocarbamate in 98% yield. According to X-ray diffraction data, the configuration of the molecule of tetraphenylantimony diethyldithiocarbamate is distorted octahedron, and the Sb-S bond lengths are 2.705(2) and 2.771(2) Angstrom.
引用
收藏
页码:1379 / 1382
页数:4
相关论文
共 7 条
[1]   E-MAP IMPROVEMENT IN DIRECT PROCEDURES [J].
ALTOMARE, A ;
CASCARANO, G ;
GIACOVAZZO, C ;
VITERBO, D .
ACTA CRYSTALLOGRAPHICA SECTION A, 1991, 47 :744-748
[2]  
[Anonymous], ACTA CRYSTALLOGR A
[3]  
Sharutin V.V., 1999, ZH OBSHCH KHIM+, V69, P1979
[4]  
Sharutin VV, 1996, ZH OBSHCH KHIM+, V66, P1755
[5]  
Sharutin VV, 1997, ZH OBSHCH KHIM+, V67, P1531
[6]  
Sharutina VV, 1997, ZH OBSHCH KHIM+, V67, P1536
[7]  
STRAVER LH, 1994, MOLEN STRUCTURE DETE, V1, P2