Properties and Rapid Low-Temperature Consolidation of Nanocrystalline Fe-ZrO2 Composite by Pulsed Current Activated Sintering

被引:32
作者
Kang, Hyun-Su [1 ]
Ko, In-Yong [1 ]
Yoon, Jin-Kook [2 ]
Doh, Jung-Mann [2 ]
Hong, Kyung-Tae [2 ]
Shon, In-Jin [1 ,3 ]
机构
[1] Chonbuk Natl Univ, Res Ctr Adv Mat Dev, Div Adv Mat Engn, Jeonju Si 561756, Jeonbuk, South Korea
[2] Korea Inst Sci & Technol, Adv Funct Mat Res Ctr, Seoul 130650, South Korea
[3] Chonbuk Natl Univ, Specialized Grad Sch, Dept Hydrogen & Fuel Cells Engn, Jeonju 561756, South Korea
关键词
mechanical alloying; composites; nanostructured material; mechanical properties; WC;
D O I
10.1007/s12540-011-0208-y
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Nanopowders of Fe and ZrO2 were synthesized from Fe2O3 and Zr by high-energy ball milling. The powder sizes of Fe and ZrO2 were 70 nm and 12 nm, respectively. Highly dense nanostructured 4/3Fe-ZrO2 composite was consolidated by a pulsed current activated sintering method within 1 minute from the mechanically synthesized powders (Fe-ZrO2) and horizontal milled Fe2O3+Zr powders under the 1 GPa pressure. The grain sizes of Fe and ZrO2 in the composite were calculated. The average hardness and fracture toughness values of nanostuctured 4/3Fe-ZrO2 composite were investigated.
引用
收藏
页码:57 / 62
页数:6
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