Interfacial microstructure of Si3N4/Si3N4 joint brazed using Au-Ni-V filler alloy

被引:7
作者
Zhang, J. [1 ]
Sun, Y. [1 ]
Liu, C. F. [1 ]
Zhang, H. W. [1 ]
机构
[1] Harbin Inst Technol, Sch Mat Sci & Engn, Harbin 150001, Peoples R China
关键词
SILICON-NITRIDE; SI3N4; STRENGTH;
D O I
10.1007/s10853-009-4132-1
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
By using Au58.74Ni36.50V4.76 at.% filler alloy, a reliable Si3N4/Si3N4 joint was brazed at 1,423 K for 60 min in vacuum. The microstructure of the joint was investigated and analyzed by scanning electron microscope with energy dispersive spectroscopy, transmission electron microscopy, and X-ray diffraction. The results indicate that the joint consists of three main phases: a continuous VN reaction layer between filler alloy and Si3N4 ceramic; an Au[Ni] solid solution as the matrix of the joint; and Ni[Si,V] solid solution particles distributed homogeneously in the Au[Ni] solid solution. The mechanism of formation of the interfacial structure is discussed.
引用
收藏
页码:2188 / 2193
页数:6
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