Synthesis and characterization of graphene-epoxy nanocomposites

被引:16
作者
Acar, Alperen [1 ]
Colak, Ozgen Umit [1 ]
Uzunsoy, Deniz [1 ]
机构
[1] Yildiz Tech Univ, Dept Mech Engn, Istanbul, Turkey
关键词
Graphene; graphene epoxy nano-composite; SEM; DMA; NANOPLATELETS; COMPOSITES; DISPERSION; BEHAVIOR;
D O I
10.3139/120.110804
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Graphene, a monolayer of carbon atoms arranged in a two dimensional lattice, has attracted great attention in recent years due to its extra ordinary properties and potential applications. One obvious application of graphene is in the field of nano-composites. In this work, graphene platelets (GPL) reinforced with epoxy nano-composites were fabricated by using soft molding technique in two different ratios with two different solvents. Raman spectroscopy and scanning electron microscopy (SEM) were used to investigate the structure of graphene and graphene reinforced composites. Tensile and dynamic mechanical analysis (DMA) in three point bending mode were used to investigate the mechanical properties of the composites. The tensile strength and strain to failure of nanocomposites of GPL reinforced epoxy nanocomposite were enhanced by 9.31 % and 34.78 %, respectively, while small improvement is observed in the elasticity modulus. Dynamic mechanical analysis has shown that with the addition of 0.1 and 0.5 wt.-% graphene nanoplatelets, storage modulus has increased by 20 and 46 % on the glassy region, respectively. The glass transition temperature is not affected with addition of graphene.
引用
收藏
页码:1001 / 1005
页数:5
相关论文
共 12 条
[1]   Effect of functionalization of graphene nanoplatelets on the mechanical response of graphene/epoxy composites [J].
Ahmadi-Moghadam, B. ;
Sharafimasooleh, M. ;
Shadlou, S. ;
Taheri, F. .
MATERIALS & DESIGN, 2015, 66 :142-149
[2]  
[Anonymous], 2010, D63810 ASTM INT
[3]   Review article: Polymer-matrix nanocomposites, processing, manufacturing, and application: An overview [J].
Hussain, Farzana ;
Hojjati, Mehdi ;
Okamoto, Masami ;
Gorga, Russell E. .
JOURNAL OF COMPOSITE MATERIALS, 2006, 40 (17) :1511-1575
[4]   Mechanical Property and Structure of Covalent Functionalised Graphene/Epoxy Nanocomposites [J].
Naebe, Minoo ;
Wang, Jing ;
Amini, Abbas ;
Khayyam, Hamid ;
Hameed, Nishar ;
Li, Lu Hua ;
Chen, Ying ;
Fox, Bronwyn .
SCIENTIFIC REPORTS, 2014, 4
[5]   Graphene nanoplatelets thickness and lateral size influence on the morphology and behavior of epoxy composites [J].
Prolongo, S. G. ;
Jimenez-Suarez, A. ;
Moriche, R. ;
Urena, A. .
EUROPEAN POLYMER JOURNAL, 2014, 53 :292-301
[6]   In situ processing of epoxy composites reinforced with graphene nanoplatelets [J].
Prolongo, S. G. ;
Jimenez-Suarez, A. ;
Moriche, R. ;
Urena, A. .
COMPOSITES SCIENCE AND TECHNOLOGY, 2013, 86 :185-191
[7]   Enhanced Mechanical Properties of Nanocomposites at Low Graphene Content [J].
Rafiee, Mohammad A. ;
Rafiee, Javad ;
Wang, Zhou ;
Song, Huaihe ;
Yu, Zhong-Zhen ;
Koratkar, Nikhil .
ACS NANO, 2009, 3 (12) :3884-3890
[8]   The effect of strain-rate on the tensile and compressive behavior of graphene reinforced epoxy/nanocomposites [J].
Shadlou, Shahin ;
Ahmadi-Moghadam, Babak ;
Taheri, Farid .
MATERIALS & DESIGN, 2014, 59 :439-447
[9]   The effect of graphene dispersion on the mechanical properties of graphene/epoxy composites [J].
Tang, Long-Cheng ;
Wan, Yan-Jun ;
Yan, Dong ;
Pei, Yong-Bing ;
Zhao, Li ;
Li, Yi-Bao ;
Wu, Lian-Bin ;
Jiang, Jian-Xiong ;
Lai, Guo-Qiao .
CARBON, 2013, 60 :16-27
[10]   Graphene filled polymer nanocomposites [J].
Verdejo, Raquel ;
Bernal, M. Mar ;
Romasanta, Laura J. ;
Lopez-Manchado, Miguel A. .
JOURNAL OF MATERIALS CHEMISTRY, 2011, 21 (10) :3301-3310