Analysis of Ergot Alkaloids

被引：61
作者：
Crews, Colin [1 ]
机构：
[1] Fera Sci Ltd, Sand Hutton YO41 1LZ, N Yorkshire, England
来源：
TOXINS | 2015年 / 7卷 / 06期
关键词：
ergot; LSD; ergotamine; lysergic acid; ergovaline; mycotoxins; LYSERGIC-ACID DIETHYLAMIDE; PERFORMANCE LIQUID-CHROMATOGRAPHY; SOLID-PHASE EXTRACTION; STAGE MASS-SPECTROMETRY; TALL FESCUE; GAS-CHROMATOGRAPHY; ISO-LSD; QUANTITATIVE-DETERMINATION; ELECTROSPRAY-IONIZATION; RYE FLOUR;
D O I：
10.3390/toxins7062024
中图分类号：
TS2 [食品工业];
学科分类号：
0832 ;
摘要：
The principles and application of established and newer methods for the quantitative and semi-quantitative determination of ergot alkaloids in food, feed, plant materials and animal tissues are reviewed. The techniques of sampling, extraction, clean-up, detection, quantification and validation are described. The major procedures for ergot alkaloid analysis comprise liquid chromatography with tandem mass spectrometry (LC-MS/MS) and liquid chromatography with fluorescence detection (LC-FLD). Other methods based on immunoassays are under development and variations of these and minor techniques are available for specific purposes.
引用
收藏
页码：2024 / 2050
页数：27
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