Synthesis of methyl-2,4-bis(cyclohexane)dispiro-1,2,3,4,4a,5,6,7-octahydro-(1H,3H)quinazoline-8-carbodithioate derived from cyclohexanone in one step

被引：7

作者：

Contreras, RR

Fontal, B ^{[1
]}

Bahsas, A

Reyes, M

Suárez, T

Bellandi, F

机构：

[1] Univ Los Andes, Fac Ciencias, Dept Quim, Lab Organomet, Merida 5101, Venezuela

[2] Univ Los Andes, Fac Ciencias, Dept Quim, Lab Nacl Resonancia Magent Nucl, Merida 5101, Venezuela

来源：

JOURNAL OF HETEROCYCLIC CHEMISTRY | 2001年 / 38卷 / 05期

关键词：

D O I：

10.1002/jhet.5570380532

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The new compound Methyl-2,4-bis(cyclohexane)dispiro-1,2,3,4,4a,5,6,7-octahydro-(1H,3H)-quinazoline-8-carbodithioate has been synthesized from cyclohexanone and carbon disulfide. It has been characterized by uv-visible, FTIR, mass spectra and a complete structure proposed based on H-1 and C-13 NMR spectroscopy.

引用

页码：1223 / 1225

页数：3

共 8 条

[1]

Bertini I., 1994, Bioinorganic Chemistry, DOI 10/BioinCh_chapter9.pdf

[2] SYNTHESIS AND ANTIFUNGAL PROPERTIES OF DITHIOCARBOXYLIC ACID DERIVAT IVES .2. NOVEL PREPARATION OF 2-ALKYLAMINO- 1-CYCLOPENTENE-1-DITHIOCARBOXYLIC ACIDS AND SOME OF THEIR DERIVATIVES [J].