A Cheap Amino Alcohol Catalyzed One-Pot, Tri-Component Synthesis of Tetrahydrochromene Derivatives

被引：12
|
作者：
Song, Shaojun [1 ]
Shan, Zixing [1 ]
Jin, Yong [1 ]
机构：
[1] Wuhan Univ, Dept Chem, Wuhan 430072, Peoples R China
来源：
LETTERS IN ORGANIC CHEMISTRY | 2010年 / 7卷 / 01期
基金：
中国国家自然科学基金;
关键词：
4H-chromene; Hantzsch reaction; one-pot synthesis; threo-(1S,2S)-2-amino-1-(4-nitrophenyl)-1,3-propanediol; MOLLUSCICIDAL-ACTIVITY; EFFICIENT SYNTHESIS; SELECTIVE OXIDATION; IONIC LIQUID; 3-COMPONENT; CHROMENE;
D O I：
10.2174/157017810790534011
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
An economic, efficient access to 4H-chromene derivatives was found. In the presence of threo-(1S,2S)-2-amino-1-(4-nitrophenyl)-1,3-propanediol, a chiral "waste" in the production of chloromycetin, and one-pot three-component Hantzsch reaction of dimedone, aldehydes and malononitrile at room temperature furnished 4H-pyran derivatives in good to excellent yield.
引用
收藏
页码：64 / 68
页数：5
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