Diaquabis(5-carboxy-2-propyl-1H-imidazole-4-carboxylato-κ2N3,O4)manganese(II) N,N-dimethylformamide disolvate

被引：13

作者：

Yan, Jian-Bin ^{[1
]}

Li, Shi-Jie ^{[1
]}

Song, Wen-Dong ^{[1
]}

Wang, Hao ^{[1
]}

Miao, Dong-Liang ^{[1
]}

机构：

[1] Guang Dong Ocean Univ, Coll Sci, Zhanjiang 524088, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷

关键词：

D O I：

10.1107/S1600536809054634

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title complex, [Mn(C8H9N2O4)(2)(H2O)(2)]center dot 2C(3)H(7)NO, the Mn-II atom, lying on an inversion centre, is six-coordinated by two N,O-bidentate 5-carboxy-2-propyl-1H-imidazole-4-carboxylate ligands and two water molecules in a distorted octahedral environment. In the crystal structure, the complex molecules and dimethylformamide solvent molecules are linked by N-H center dot center dot center dot O and O-H center dot center dot center dot O hydrogen bonds into a two-dimensional supramolecular network parallel to (001).

引用

页码：M99 / U1026

页数：10

共 7 条

[1]

Bruker, 2007, APEX2 SAINT

[2] Syntheses and characterizations of two novel Ln(III)-Cu(II) coordination polymers constructed by pyridine-2,4-dicarboxylate ligand [J].

Liang, YC ;

Cao, R ;

Hong, MC ;

Sun, DF ;

Zhao, YJ ;

Weng, JB ;

Wang, RH .

INORGANIC CHEMISTRY COMMUNICATIONS, 2002, 5 (05) :366-368

[3] NOVEL STACKING IN A BINUCLEAR IRIDIUM CARBONYL IMIDAZOLEDICARBOXYLATE [J].

NET, G ;

BAYON, JC ;

BUTLER, WM ;

RASMUSSEN, P .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1989, (15) :1022-1023

[4] Diaquabis(5-carboxy-2-methyl-1H-imidazole-4-carboxylato-κ2,N3,O4)cadmium(II) [J].

Nie, Xu-Liang ;

Wen, Hui-Liang ;

Wu, Zi-Sheng ;

Liu, Da-Bo ;

Liu, Chong-Bo .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 :m753-m755

[5]

Sheldrick G.M., 1996, SADABS

[6] A short history of SHELX [J].

Sheldrick, George M. .

ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122

[7] Poly[diaquabis(μ-4-carboxy-2-propyl-1H-imidazole-5-carboxylato-κ3N3,O4:O5)calcium(II)] [J].

Song, Wen-Dong ;

Yan, Jian-Bin ;

Li, Shi-Jie ;

Miao, Dong-Liang ;

Li, Xiao-Fei .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 :M53-U604

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