Adiabatic dipolar recoupling in solid-state NMR: The DREAM scheme

被引：173
|
作者：
Verel, R [1 ]
Ernst, M [1 ]
Meier, BH [1 ]
机构：
[1] ETH Honggerberg, Chem Phys Lab, CH-8093 Zurich, Switzerland
来源：
JOURNAL OF MAGNETIC RESONANCE | 2001年 / 150卷 / 01期
关键词：
D O I：
10.1006/jmre.2001.2310
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
A theoretical treatment of the DREAM adiabatic homonuclear recoupling experiment is given using Floquet theory. An effective Hamiltonian is derived analytically and the time evolution of the density operator in the adiabatic limit is described. Shape cycles are proposed and characterized experimentally. Application to spin-pair filtering and as a mixing period in a 2D correlation experiment is explored and the experimental results are compared to theoretical predictions and exact numerical simulations. (C) 2001 Academic Press.
引用
收藏
页码：81 / 99
页数：19
相关论文
共 50 条
  • [1] Improving solid-state NMR dipolar recoupling by optimal control
    Kehlet, CT
    Sivertsen, AC
    Bjerring, M
    Reiss, TO
    Khaneja, N
    Glaser, SJ
    Nielsen, NC
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2004, 126 (33) : 10202 - 10203
  • [2] Improving solid-state NMR dipolar recoupling by optimal control
    1600, American Chemical Society, Columbus, United States (126):
  • [3] Dipolar recoupling in fast-MAS solid-state NMR spectroscopy
    Schnell, I
    PROGRESS IN NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY, 2004, 45 (1-2) : 145 - 207
  • [4] Improved transfer efficiencies in radio-frequency-driven recoupling solid-state NMR by adiabatic sweep through the dipolar recoupling condition
    Straaso, Lasse A.
    Shankar, Ravi
    Tan, Kong Ooi
    Hellwagner, Johannes
    Meier, Beat H.
    Hansen, Michael Ryan
    Nielsen, Niels Chr.
    Vosegaard, Thomas
    Ernst, Matthias
    Nielsen, Anders B.
    JOURNAL OF CHEMICAL PHYSICS, 2016, 145 (03):
  • [5] Enhanced symmetry-based dipolar recoupling in solid-state NMR
    Edén, M
    CHEMICAL PHYSICS LETTERS, 2003, 378 (1-2) : 55 - 64
  • [6] Overcoming Volume Selectivity of Dipolar Recoupling in Biological Solid-State NMR Spectroscopy
    Tosner, Zdenek
    Sarkar, Riddhiman
    Becker-Baldus, Johanna
    Glaubitz, Clemens
    Wegner, Sebastian
    Engelke, Frank
    Glaser, Steffen J.
    Reif, Bernd
    ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2018, 57 (44) : 14514 - 14518
  • [7] Multidimensional dipolar exchange-assisted recoupling measurements in solid-state NMR
    Sachleben, JR
    Beverwyk, P
    Frydman, L
    JOURNAL OF MAGNETIC RESONANCE, 2000, 144 (02) : 330 - 342
  • [8] Distance measurements by dipolar recoupling two-dimensional solid-state NMR
    Kiihne, S
    Mehta, MA
    Stringer, JA
    Gregory, DM
    Shiels, JC
    Drobny, GP
    JOURNAL OF PHYSICAL CHEMISTRY A, 1998, 102 (13): : 2274 - 2282
  • [9] Theory of frequency-selective homonuclear dipolar recoupling in solid-state NMR
    Xiao, Hang
    Zhang, Zhengfeng
    Yang, Jun
    JOURNAL OF CHEMICAL PHYSICS, 2021, 155 (17):
  • [10] Broadband dipolar recoupling for magnetization transfer in solid-state NMR correlation spectroscopy
    Duma, Luminita
    Abergel, Daniel
    Ferrage, Fabien
    Pelupessy, Philippe
    Tekely, Piotr
    Bodenhausen, Geoffrey
    CHEMPHYSCHEM, 2008, 9 (08) : 1104 - 1106
12345