MODERN TECHNIQUES OF SAMPLE PREPARATION FOR PESTICIDE RESIDUES DETERMINATION IN WATER BY LIQUID CHROMATOGRAPHY WITH DETECTION BY DIODE ARRAY AND MASS SPECTROMETRY

被引：54

作者：

Caldas, Sergiane Souza ^{[1
]}

Goncalves, Fabio Ferreira ^{[1
]}

Primel, Ednei Gilberto ^{[1
]}

Prestes, Osmar Damian ^{[2
]}

Martins, Manoel Leonardo ^{[2
]}

Zanella, Renato ^{[2
]}

机构：

[1] Univ Fed Rio Grande, Escola Quim & Alimentos, BR-96201900 Rio Grande, RS, Brazil

[2] Univ Fed Santa Maria, Dept Quim, BR-97105900 Santa Maria, RS, Brazil

来源：

QUIMICA NOVA | 2011年 / 34卷 / 09期

关键词：

extraction; pesticides; water; SOLID-PHASE EXTRACTION; BAR SORPTIVE EXTRACTION; LC-MS-MS; ULTRA-TRACE QUANTIFICATION; PHENOXY ACIDIC PESTICIDES; PADDY-FIELD WATER; SURFACE WATERS; ORGANOCHLORINE PESTICIDES; AQUEOUS SAMPLES; ORGANOPHOSPHORUS PESTICIDES;

D O I：

10.1590/S0100-40422011000900021

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

MODERN TECHNIQUES OF SAMPLE PREPARATION FOR PESTICIDE RESIDUES DETERMINATION IN WATER BY LIQUID CHROMATOGRAPHY WITH DETECTION BY DIODE ARRAY AND MASS SPECTROMETRY. The determination of pesticide residues in water samples by Liquid Chromatography require sample preparation for extraction and enrichment of the analytes with the minimization of interferences to achieve adequate detection limits. The Solid Phase Extraction (SPE), Solid Phase Microextraction (SPME), Stir Bar Sorptive Extraction (SBSE) and Dispersive Liquid-Liquid Microextraction (DLLME) techniques have been widely used for extraction of pesticides in water. In this review, the principles of these sample preparation techniques associated with the analysis by Liquid Chromatography with Diode Array Detection (LC-DAD) or Mass Spectrometry (LC-MS) are described and an overview of several applications were presented and discussed.

引用

页码：1604 / 1617

页数：14

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