Pesticide residues in fruits and vegetables in Jordan using liquid chromatography/tandem mass spectrometry

被引：42

作者：

Algharibeh, Ghaith Radwan ^{[1
]}

AlFararjeh, Malik Salah ^{[1
]}

机构：

[1] Jordan Food & Drug Adm, Food Lab, Contaminants Monitoring Div, Amman, Jordan

来源：

FOOD ADDITIVES & CONTAMINANTS PART B-SURVEILLANCE | 2019年 / 12卷 / 01期

关键词：

Fruits; Jordan; LC-MS; MS; pesticides; QuEchERS; vegetables; HEALTH-RISK ASSESSMENT; MULTIRESIDUE METHOD; SAMPLE PREPARATION; QUECHERS; EXTRACTION; FOODS;

D O I：

10.1080/19393210.2018.1548505

中图分类号：

O69 [应用化学];

学科分类号：

081704 ;

摘要：

A total of 158 fruit and vegetable samples produced in Jordan were examined for the presence of pesticide residues using the multi-residue analysis technique by Liquid Chromatography-tandem Mass Spectrometry (LC-MS/MS) and the QuEchERS extraction method. A total of 73 samples (46%) were free from detectable residues, while 85 samples (54%) contained residues. Among the tested samples, 34 (22%) contained residues above Maximum Residue Levels (MRLs) and 51 (32%) contained residues at or below MRLs. Most of the detected residues were found in sweet pepper, peach and apricot samples. Only watermelon samples were free from detectable residues, while tomato and melon samples exhibited residues below MRLs. Out of the 113 pesticides tested, 22 pesticides were found above the limit of detection, 9 of which (hexaconazole, propargite, propiconazole, myclobutanil, thiamethoxam, thiacloprid, clothianidin, clofentezine and pyridaben) had residues that violate MRLs according to European regulations. A continuous monitoring programme for pesticide residues in Jordanian fruits and vegetables is highly recommended.

引用

页码：65 / 73

页数：9

共 32 条

[1]

Afify AEMMR, 2010, J FOOD AGRIC ENVIRON, V8, P602

[2] Occurrence of organochlorine pesticide residues in eggs, chicken and meat in Jordan [J].

Ahmad, Rafat ;

Salem, Nida' M. ;

Estaitieh, Hussein .

CHEMOSPHERE, 2010, 78 (06) :667-671

[3] Analyses of pesticides and their metabolites in foods and drinks [J].

Ahmed, FE .

TRAC-TRENDS IN ANALYTICAL CHEMISTRY, 2001, 20 (11) :649-661

[4] Pesticides and trace metals residue in grape and home made wine in Jordan [J].

Al Nasir, FM ;

Jiries, AG ;

Batarseh, MI ;

Beese, F .

ENVIRONMENTAL MONITORING AND ASSESSMENT, 2001, 66 (03) :253-263

[5] Increased occurrence of pesticide residues on crops grown in protected environments compared to crops grown in open field conditions [J].

Allen, Gina ;

Halsall, Crispin J. ;

Ukpebor, Justina ;

Paul, Nigel D. ;

Ridall, Gareth ;

Wargent, Jason J. .

CHEMOSPHERE, 2015, 119 :1428-1435

[6]

Anastassiades M, 2003, J AOAC INT, V86, P412

[7]

[Anonymous], 2008, European standard E N 15662, Foods of Plant Origin-Determination of Pesticide Residues Using GC-MS And/Or LC-MS/MS Following Acetonitrile Extraction/Partitioning and Clean-Up by Dispersive SPE-QuechERS-Method

[8]

[Anonymous], 2005, Official Journal of the European Union, L, V70/, P1

[9] Surveillance of pesticide residues in fruits from Valencia during twenty months (2004/05) [J].

Berrada, H. ;

Fernandez, M. ;

Ruiz, M. J. ;

Molto, J. C. ;

Manes, J. ;

Font, G. .

FOOD CONTROL, 2010, 21 (01) :36-44

[10] Contamination of vegetables of different seasons with organophosphorous pesticides and related health risk assessment in northern India [J].

Bhanti, Mayank ;

Taneia, Ajay .

CHEMOSPHERE, 2007, 69 (01) :63-68

← 1 2 3 4 →