STRUCTURAL AND MAGNETIC PROPERTIES OF ZINC DOPED COPPER FERRITE SYNTHESIZED BY SOL-GEL AND HYDROTHERMAL ROUTE

被引:6
|
作者
Kumar, Naveen [1 ]
Singh, Deepak [1 ]
Nigam, Abhishek [1 ]
Rajpoot, Omprakash [1 ]
Yadav, Mayank Kumar [1 ]
Singh, Yogendra Pratap [1 ]
Prakash, P. Shakti [1 ]
Singh, Samarjit [1 ]
机构
[1] Motilal Nehru Natl Inst Technol Allahabad, Appl Mech Dept, Prayagraj 211004, India
来源
MATERIALS PHYSICS AND MECHANICS | 2021年 / 47卷 / 02期
关键词
copper; hydrothermal; sol-gel; spinel ferrite; zinc; ELECTRICAL-PROPERTIES; NANOPARTICLES;
D O I
10.18149/MPM.4722021_12
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Y In this work, Cu-Zn spinel ferrites having chemical formula Cu(1-x)ZnxFe2O4 for x ranging from 0.2 to 0.8 were synthesized by sol-gel auto-combustion method and hydrothermal method with a step size of 0.2. The effect of Zn doping on structural properties, crystallite size, and magnetic properties synthesized by both methods are reported. Rietveld refinement of the XRD patterns was analyzed using Maud for the determination of crystallite size. The X-ray diffraction pattern shows that single phase Cu-Zn spinel ferrite was formed, and it has a cubic structure. Additionally, the lattice parameter size increases with Zn doping and then decreases after x=0.6. A vibrating sample magnetometer (VSM) was done to determine magnetic properties like saturation magnetization (Ms), remanence (Mr), and coercivity (Hc). The scanning electron microscopy (SEM) shows the morphology and confirms the average particle size.
引用
收藏
页码:306 / 314
页数:9
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