Effects of quenching process on microstructure, mechanical properties and magnetic susceptibility in Zr-1Mo alloy fabricated by powder bed fusion process

被引:13
作者
Sun, Xiaohao [1 ,2 ]
Liu, Debao [1 ]
Zhou, Weiwei [2 ]
Nomura, Naoyuki [2 ]
Doi, Hisashi [3 ]
Tsutsumi, Yusuke [3 ,4 ]
Hanawac, Takao [3 ]
机构
[1] Tianjin Univ Technol, Sch Mat Sci & Engn, Tianjin 300384, Peoples R China
[2] Tohoku Univ, Grad Sch Engn, Dept Mat Proc, Sendai, Miyagi 9808579, Japan
[3] Tokyo Med & Dent Univ, Inst Biomat & Bioengn, Tokyo 1010062, Japan
[4] Natl Inst Mat Sci, Res Ctr Struct Mat, Ibaraki 3050047, Japan
关键词
Powder bed fusion process; Zr-based alloy; Quenching process; Microstructure; Magnetic resonance imaging compatibility; RESIDUAL-STRESS; HEAT-TREATMENT; ARTIFACTS; MO; TI-6AL-4V; MRI; AU; CU;
D O I
10.1016/j.matdes.2019.108356
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In order to depress the "susceptibility artifacts" in magnetic resonance imaging (MRI), improve the mechanical reliability for biomedical structural applications and realize tailor-made medical devices with complex shape, low magnetic Zr-1 Mo(wt%) alloy builds with high relative density (c.a.99.9%) fabricated by laser powder bed fusion process(L-PBF) were subjected to various heat treatment conditions followed by water quenching. After quenching process acicular alpha' microsturcture in as-build Zr-1Mo(wt%) alloy builds changed to basket weave alpha + beta structure, unique retained alpha + ultra fine (alpha' + alpha '') martensite structure or retained alpha + acicular alpha' microsturcture depending on quenching conditions. X-ray diffraction (XRD) and high resolution-transmission electron microscope(HR-TEM) revealed a unique retained alpha + ultra fine (alpha' + alpha '') martensite microstructure in 1123 K specimens. The stress-induced competition between beta to alpha' transformation and beta to alpha '' transformation contributed to this unique microstructure. This unique microstructure contributed to a good balance between strength (IHS:822 MPa) and ductility (Elongation:11.7%). The volume magnetic susceptibility of quenched Zr1 Mo(wt%) alloy builds maintained low(about 1.01 x 10(-4) ) indicating good MRI compatibility. The magnetic susceptibility of each phase was modified to be chi(alpha '')> chi(beta) >chi(alpha) > chi(alpha') > chi(omega) Zr-1Mo(wt%) alloy quenched from 1123 K will be an promising candidates for tailor made devices under MRI environments. (C) 2018 The Authors. Published by Elsevier Ltd.
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页数:11
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