Evaluation of fracture toughness of small volumes by means of cube-corner nanoindentation

被引:47
作者
Cuadrado, N. [1 ]
Casellas, D. [1 ,2 ]
Anglada, M. [3 ]
Jimenez-Pique, E. [3 ]
机构
[1] Fundacio CTM Ctr Tecnol, Manresa 08242, Spain
[2] Univ Politecn Cataluna, Dept Mat Sci & Met Engn, EPSEM, Manresa 08242, Spain
[3] Univ Politecn Cataluna, Dept Mat Sci & Met Engn, ETSEIB, E-08028 Barcelona, Spain
关键词
Nanoindentation; Fracture toughness; Cube-corner indenter; Crack morphology; INDENTATION FRACTURE; MECHANICAL-PROPERTIES; SINGLE-CRYSTAL; THIN-FILMS; GLASS; COATINGS; CRACKING; LOAD; SI;
D O I
10.1016/j.scriptamat.2012.01.033
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
In this work, the applicability of the two most commonly used equations for calculating the fracture toughness by nanoindentation is discussed in terms of indenter geometry and indentation crack morphology. These equations are calibrated for Berkovich and cube-corner indenters taking into account the actual indentation crack morphology, in order to attain a more reliable estimation of fracture toughness in small material volumes by nanoindentation. (C) 2012 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
引用
收藏
页码:670 / 673
页数:4
相关论文
共 23 条
[1]   A CRITICAL-EVALUATION OF INDENTATION TECHNIQUES FOR MEASURING FRACTURE-TOUGHNESS .1. DIRECT CRACK MEASUREMENTS [J].
ANSTIS, GR ;
CHANTIKUL, P ;
LAWN, BR ;
MARSHALL, DB .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1981, 64 (09) :533-538
[2]  
Bull S.J., 2011, CR MECANIQUE, V339, P5178
[3]   Fracture toughness of carbides in tool steels evaluated by nanoindentation [J].
Casellas, Daniel ;
Caro, Jaume ;
Molas, Silvia ;
Prado, Jose M. ;
Valls, Isaac .
ACTA MATERIALIA, 2007, 55 (13) :4277-4286
[4]   Indentation fracture and toughness assessment for thin optical coatings on glass [J].
Chen, J. ;
Bull, S. J. .
JOURNAL OF PHYSICS D-APPLIED PHYSICS, 2007, 40 (18) :5401-5417
[5]   COMPARATIVE MEASUREMENT OF INDENTATION FRACTURE-TOUGHNESS WITH BERKOVICH AND VICKERS INDENTERS [J].
DUKINO, RD ;
SWAIN, MV .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1992, 75 (12) :3299-3304
[6]   Fracture anisotropy in silicon single crystal [J].
Ebrahimi, F ;
Kalwani, L .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 1999, 268 (1-2) :116-126
[7]  
HARDING DS, 1995, MATER RES SOC SYMP P, V356, P663, DOI 10.1557/PROC-356-663
[8]   THE MEASUREMENT OF KIC IN SINGLE-CRYSTAL SIC USING THE INDENTATION METHOD [J].
HENSHALL, JL ;
BROOKES, CA .
JOURNAL OF MATERIALS SCIENCE LETTERS, 1985, 4 (06) :783-786
[9]   Influence of indenter angle on cracking in Si and Ge during nanoindentation [J].
Jang, Jae-il ;
Pharr, G. M. .
ACTA MATERIALIA, 2008, 56 (16) :4458-4469
[10]   Indentation fracture toughness and acoustic energy release in tetrahedral amorphous carbon diamond-like thin films [J].
Jungk, J. M. ;
Boyce, B. L. ;
Buchheit, T. E. ;
Friedmann, T. A. ;
Yang, D. ;
Gerberich, W. W. .
ACTA MATERIALIA, 2006, 54 (15) :4043-4052