New Clean-up Method with Dispersive Solid-Phase Extraction for Simultaneous Determination of Pesticide Residues in Livestock Products by GC-MS/MS

被引：6
|
作者：
Kondo, Takahide [1 ]
Kaburagi, Yasuo [1 ]
Shibata, Masahisa [1 ]
Kurokawa, Chieko [1 ]
Inoue, Yutaka [1 ]
Yamamoto, Yoshihiko [2 ]
Miyazaki, Motonobu [1 ]
机构：
[1] Saitama City Inst Hlth Sci & Res, Div Life Sci, Chuo Ku, Saitama 3380013, Japan
[2] Sendai Med Ctr, Natl Hlth Org, Miyagino Ku, Sendai, Miyagi 9830045, Japan
来源：
FOOD HYGIENE AND SAFETY SCIENCE | 2012年 / 53卷 / 02期
关键词：
livestock products; pesticide residues; simultaneous determination; dispersive solid-phase extraction; multifunctional column; refrigerated centrifugation; gas chromatography-tandem mass spectrometry (GC-MS/MS);
D O I：
10.3358/shokueishi.53.75
中图分类号：
TS2 [食品工业];
学科分类号：
0832 ;
摘要：
A simple clean-up method was developed for the simultaneous determination of pesticide residues in livestock products by GC-MS/MS. The pesticide residues were extracted with acetonitrile ethanol (1: 1), and matrix components such as adipose were effectively eliminated by a combination of refrigerated centrifugation, dispersive solid-phase extraction, and multifunctional column chromatography. In this method, samples are treated quickly and easily without the need for gel-permeation chromatography. Among 131 pesticides tested, 115 showed recovery within the range from 70 to 120%, with relative standard deviations of less than 15%. The quantification limits for the 115 pesticides in livestock products were 0.001 to 0.01 mu g/g.
引用
收藏
页码：75 / 84
页数：10
相关论文
共 50 条
  • [1] An evaluation method for determination of non-polar pesticide residues in animal fat samples by using dispersive solid-phase extraction clean-up and GC-MS
    Mercedes Castillo
    Carmen González
    Ana Miralles
    Analytical and Bioanalytical Chemistry, 2011, 400 : 1315 - 1328
  • [2] An evaluation method for determination of non-polar pesticide residues in animal fat samples by using dispersive solid-phase extraction clean-up and GC-MS
    Castillo, Mercedes
    Gonzalez, Carmen
    Miralles, Ana
    ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2011, 400 (05) : 1315 - 1328
  • [3] A Simultaneous Determination Method with Acetonitrile-n-Hexane Partitioning and Solid-Phase Extraction for Pesticide Residues in Livestock and Marine Products by GC-MS
    Yoshizaki, Mayuko
    Kobayashi, Yukari
    Shimizu, Masanori
    Maruyama, Kouichi
    FOOD HYGIENE AND SAFETY SCIENCE, 2015, 56 (03): : 77 - 82
  • [4] Determination of 66 pesticide residues in livestock products using QuEChERS and GC-MS/MS
    Kang, Hye Soon
    Kim, MeeKyung
    Kim, Eun Jeong
    Choe, Won-Jo
    FOOD SCIENCE AND BIOTECHNOLOGY, 2020, 29 (11) : 1573 - 1586
  • [5] Dispersive solid-phase extraction clean up combined with Soxhlet extraction for the determination of 16 PAHs in soil samples by GC-MS
    Nikolic, Jelena S.
    Jovanovic, Vesna P. Stankov
    Dimitrijevic, Marija V.
    Cvetkovic, Dragan J.
    Stanojevic, Ljiljana P.
    Nikolic, Ljubisa B.
    Mitic, Violeta D.
    INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 2017, 97 (02) : 112 - 123
  • [6] Optimization of Clean-up Process Conditions by Comparative Analysis of Dispersive Solid Phase Extraction and Automated Micro Solid Phase Extraction Clean-up for GC-MS/MS Analysis of Pesticides in Tuber Crops
    Singh, Sarvendra Pratap
    Sharma, Jyoti
    ANALYTICAL CHEMISTRY LETTERS, 2021, 11 (01) : 29 - 38
  • [7] Solid phase extraction (SPE) of pesticide residues in fruits followed by GC-MS determination
    Branca, P
    Sacchero, G
    INDUSTRIE ALIMENTARI, 1997, 36 (358): : 482 - 488
  • [8] Determination of 400 pesticide residues in green tea leaves by UPLC-MS/MS and GC-MS/MS combined with QuEChERS extraction and mixed-mode SPE clean-up method
    Ly, Tuan-Kiet
    Ho, Tuan-Dat
    Behra, Philippe
    Nhu-Trang, Tran-Thi
    FOOD CHEMISTRY, 2020, 326
  • [9] Simultaneous determination of 36 pesticide residues in spinach and cauliflower by LC-MS/MS using multi-walled carbon nanotubes-based dispersive solid-phase clean-up
    Fan, Sufang
    Zhao, Pengyue
    Yu, Chuanshan
    Pan, Canping
    Li, Xuesheng
    FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT, 2014, 31 (01): : 73 - 82
  • [10] An effective method for pesticide residues determination in tobacco by GC-MS/MS and UHPLC-MS/MS employing acetonitrile extraction with low-temperature precipitation and d-SPE clean-up
    Bernardi, Gabrieli
    Kemmerich, Magali
    Ribeiro, Lucila C.
    Adaime, Martha B.
    Zanella, Renato
    Prestes, Osmar D.
    TALANTA, 2016, 161 : 40 - 47
12345