Peak measurement and calibration in chromatographic analysis

被引:15
作者
Asnin, Leonid D. [1 ]
机构
[1] Perm Natl Res Polytech Univ, Dept Chem & Biotechnol, Perm 614990, Russia
关键词
Calibration; Chromatography; Quantitative analysis; Peak detection; Peak integration; Inverse calibration; TANDEM MASS-SPECTROMETRY; PERFORMANCE LIQUID-CHROMATOGRAPHY; LIGHT-SCATTERING DETECTION; GAS-CHROMATOGRAPHY; HUMAN PLASMA; INTERNAL STANDARD; METHOD VALIDATION; AUTOMATED-METHOD; LEAST-SQUARES; DETECTOR;
D O I
10.1016/j.trac.2016.01.006
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The precision and accuracy of quantitative chromatographic analysis depends significantly on the quality of calibration. This review considers such aspects of the calibration procedure as design of a calibration experiment, choice of a calibration model, and regression analysis of calibration data. A brief description of the theory of chromatographic detection and modern approaches to data acquisition and processing is given in the context of the calibration problem. (C) 2016 Elsevier B.V. All rights reserved.
引用
收藏
页码:51 / 62
页数:12
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