Peak measurement and calibration in chromatographic analysis

被引:19
作者
Asnin, Leonid D. [1 ]
机构
[1] Perm Natl Res Polytech Univ, Dept Chem & Biotechnol, Perm 614990, Russia
关键词
Calibration; Chromatography; Quantitative analysis; Peak detection; Peak integration; Inverse calibration; TANDEM MASS-SPECTROMETRY; PERFORMANCE LIQUID-CHROMATOGRAPHY; LIGHT-SCATTERING DETECTION; GAS-CHROMATOGRAPHY; HUMAN PLASMA; INTERNAL STANDARD; METHOD VALIDATION; AUTOMATED-METHOD; LEAST-SQUARES; DETECTOR;
D O I
10.1016/j.trac.2016.01.006
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The precision and accuracy of quantitative chromatographic analysis depends significantly on the quality of calibration. This review considers such aspects of the calibration procedure as design of a calibration experiment, choice of a calibration model, and regression analysis of calibration data. A brief description of the theory of chromatographic detection and modern approaches to data acquisition and processing is given in the context of the calibration problem. (C) 2016 Elsevier B.V. All rights reserved.
引用
收藏
页码:51 / 62
页数:12
相关论文
共 85 条
[1]   A universal denoising and peak picking algorithm for LC-MS based on matched filtration in the chromatographic time domain [J].
Andreev, VP ;
Rejtar, T ;
Chen, HS ;
Moskovets, EV ;
Ivanov, AR ;
Karger, BL .
ANALYTICAL CHEMISTRY, 2003, 75 (22) :6314-6326
[2]  
[Anonymous], 2004, MODERN PRACTICE GAS, DOI DOI 10.1002/0471651141
[3]  
[Anonymous], 2014, AG OPENLAB CDS CHEMS
[4]  
[Anonymous], 2013, GUID IND BIOAN METH
[5]   A simple peak detection and label-free quantitation algorithm for chromatography-mass spectrometry [J].
Aoshima, Ken ;
Takahashi, Kentaro ;
Ikawa, Masayuki ;
Kimura, Takayuki ;
Fukuda, Mitsuru ;
Tanaka, Satoshi ;
Parry, Howell E. ;
Fujita, Yuichiro ;
Yoshizawa, Akiyasu C. ;
Utsunomiya, Shin-ichi ;
Kajihara, Shigeki ;
Tanaka, Koichi ;
Oda, Yoshiya .
BMC BIOINFORMATICS, 2014, 15
[6]   Calibration of a detector for nonlinear responses [J].
Asnin, L ;
Guiochon, G .
JOURNAL OF CHROMATOGRAPHY A, 2005, 1089 (1-2) :105-110
[7]   Calibration of detector responses using the shape and size of band profiles - Case of a nonlinear response curve [J].
Asnin, L ;
Guiochon, G .
JOURNAL OF CHROMATOGRAPHY A, 2005, 1089 (1-2) :101-104
[8]   Calibration of a detector for nonlinear chromatography [J].
Asnin, L ;
Galinada, W ;
Götmar, G ;
Guiochon, G .
JOURNAL OF CHROMATOGRAPHY A, 2005, 1076 (1-2) :141-147
[9]  
Beesley T.E., 2001, Quantitative chromatographic analysis
[10]   An analysis of the SFSTP guide on validation of chromatographic bioanalytical methods: progresses and limitations [J].
Boulanger, B ;
Chiap, P ;
Dewe, W ;
Crommen, J ;
Hubert, P .
JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 2003, 32 (4-5) :753-765