Influence of the focus offset on the defects, microstructure, and mechanical properties of an Inconel 718 superalloy fabricated by electron beam additive manufacturing

被引:41
作者
Lee, Hae-Jin [1 ]
Kim, Han-Kyu [2 ]
Hong, Hyun-Uk [2 ]
Lee, Byoung-Soo [1 ]
机构
[1] Korea Inst Ind Technol KITECH, Addit Mfg Proc R&D Grp, Gwahakdanji Ro 134-41, Kangnung 25440, Gangwon Do, South Korea
[2] Changwon Natl Univ, Dept Mat Sci & Engn, 20 Changwondaehak Ro, Chang Won 51140, Gyeongnam, South Korea
关键词
Additive manufacturing; Nickel-based superalloys; Focus offset; Columnar grain microstructure; gamma '/gamma ''/gamma ' Sandwich structures; HEAT-TREATMENT; TENSILE BEHAVIOR; COOLING RATES; LASER; ALLOY; PRECIPITATION; DELTA; EVOLUTION;
D O I
10.1016/j.jallcom.2018.12.070
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
The defects, microstructure, and mechanical properties of Inconel 718 superalloy fabricated by electron beam additive manufacturing with different focus offsets were investigated. The samples built with a low focus offset exhibited numerous micro-voids of 10 mu m and a columnar grain microstructure with a strong [001] texture in the built direction (BD). Unmelted powder and macro-voids of approximately 200 mu m were observed at higher focus offsets, and the columnar grain width decreased from 600 mu m to 150 mu m with increasing focus offset. gamma' precipitates with a length of 10 nm developed parallel to the BD, while gamma '' precipitates with length of 4 nm formed perpendicular to the BD owing to the higher thermal conductivity. Samples built with a low focus offset exhibited intergranular fractures, while samples built with a high focus offset exhibited brittle fractures because of the unmelted powder and macro-voids. Samples built with focus offsets of 9 mA and 12 mA exhibited the highest tensile strengths of 1.3 GPa and 1.0 GPa at room temperature and high temperature, respectively.gamma'/gamma ''/gamma' and gamma'/gamma ''/gamma'/gamma ''/gamma' sandwich structures on the columnar gamma grains developed parallel to the BD in the as-built samples because the preheating process between consecutive layers increases the dwelling time in the temperature range facilitating the delta -> gamma '' and delta -> gamma' phase transformation. The volume fractions and size of the gamma' and gamma '' precipitates increase with the focus offset owing to the prolonged dwelling time; however, micro-voids formed and unmelted powder was present because of insufficient heat of fusion. (C) 2018 Elsevier B.V. All rights reserved.
引用
收藏
页码:842 / 856
页数:15
相关论文
共 53 条
[1]   Selective Growth of Low Stored Energy Grains During δ Sub-solvus Annealing in the Inconel 718 Nickel-Based Superalloy [J].
Agnoli, Andrea ;
Bernacki, Marc ;
Loge, Roland ;
Franchet, Jean-Michel ;
Laigo, Johanne ;
Bozzolo, Nathalie .
METALLURGICAL AND MATERIALS TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE, 2015, 46A (09) :4405-4421
[2]   Precipitation and clustering in the early stages of ageing in Inconel 718 [J].
Alam, Talukder ;
Chaturvedi, Mahesh ;
Ringer, Simon P. ;
Cairney, Julie M. .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2010, 527 (29-30) :7770-7774
[3]   Microstructures and mechanical behavior of Inconel 718 fabricated by selective laser melting [J].
Amato, K. N. ;
Gaytan, S. M. ;
Murr, L. E. ;
Martinez, E. ;
Shindo, P. W. ;
Hernandez, J. ;
Collins, S. ;
Medina, F. .
ACTA MATERIALIA, 2012, 60 (05) :2229-2239
[4]  
[Anonymous], 2000, Electron Backscatter Diffraction in Materials Science
[5]  
[Anonymous], ADV ENG MAT
[6]  
ASTM, 2014, F305512 ASTM INT
[7]   On the microstructural and mechanical properties of post-treated additively manufactured Inconel 718 superalloy under quasi-static and cyclic loading [J].
Aydinoez, M. E. ;
Brenne, F. ;
Schaper, M. ;
Schaak, C. ;
Tillmann, W. ;
Nellesen, J. ;
Niendorf, T. .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2016, 669 :246-258
[8]   Absence of dynamic strain aging in an additively manufactured nickel-base superalloy [J].
Beese, Allison M. ;
Wang, Zhuqing ;
Stoica, Alexandru D. ;
Ma, Dong .
NATURE COMMUNICATIONS, 2018, 9
[9]   In-situ characterization of laser-powder interaction and cooling rates through high-speed imaging of powder bed fusion additive manufacturing [J].
Bertoli, Umberto Scipioni ;
Guss, Gabe ;
Wu, Sheldon ;
Matthews, Manyalibo J. ;
Schoenung, Julie M. .
MATERIALS & DESIGN, 2017, 135 :385-396
[10]   Producing Ni-base superalloys single crystal by selective electron beam melting [J].
Chauvet, Edouard ;
Tassin, Catherine ;
Blandin, Jean-Jacques ;
Dendievel, Remy ;
Martin, Guilhem .
SCRIPTA MATERIALIA, 2018, 152 :15-19