Total assignment of 1H and 13C NMR spectra of 13α- and 13β-estrone methyl ethers

被引：9

作者：

Ciuffreda, P

Ferraboschi, P

Verza, E

Manzocchi, A

机构：

[1] Univ Milan, Dipartimento Chim & Biochim Med, I-20133 Milan, Italy

[2] Univ Milan, Dipartimento Sci Preclin LITA Vialba, I-20157 Milan, Italy

来源：

MAGNETIC RESONANCE IN CHEMISTRY | 2001年 / 39卷 / 10期

关键词：

NMR; H-1; C-13; 1D HOHAHA; COSY; NOESY; TOCSY; HSQC; steroids; estrone methyl ether; 13; alpha-epimer;

D O I：

10.1002/mrc.891

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The complete H-1 and C-13 chemical shift assignments of the 13 alpha -epimer of estrone methyl ether and of estrone methyl ether itself were carried out, making use of one- and two-dimensional NMR techniques (1D HOHAHA, COSY, NOESY, TOCSY and HSQC). Copyright (C) 2001 John Wiley & Sons, Ltd.

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页码：648 / 650

页数：3

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