Co-crystallization of oxadiazole-bridged pyridyl-N-oxide building modules with R-aromatics (R = -OH, -NH2 and -COOH)

被引：32
作者：
Hou, Gui-Ge [1 ]
Ma, Jian-Ping [1 ]
Wang, Le [1 ]
Wang, Ping [1 ]
Dong, Yu-Bin [1 ]
Huang, Ru-Qi [1 ]
机构：
[1] Shandong Normal Univ, Coll Chem Chem Engn & Mat Sci, Engn Res Ctr Pesticide & Med Intermediate Clean P, Key Lab Mol & Nano Probe,Minist Educ, Jinan 250014, Peoples R China
来源：
CRYSTENGCOMM | 2010年 / 12卷 / 12期
关键词：
TUNABLE LUMINESCENT PROPERTIES; ORGANIC ROTAXANE FRAMEWORKS; BENZOIC-ACID DERIVATIVES; COORDINATION POLYMERS; HYDROGEN-BOND; TRIMESIC ACID; CRYSTALS; COMPLEXES; 3D; DESIGN;
D O I：
10.1039/b923810g
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The reaction of oxadiazole bridging pyridyl-N-oxides (2,5-bis(4-pyridyl-N-oxide)-1,3,4-oxadiazole (A1) and 2-(4-pyridyl)-5-(4-pyridyl-N-oxide)-1,3,4-oxadiazole (A2)) with different substituted aromatics (R-aromatics, R = -OH, -NH2, -COOH) have been investigated. Eight new organic co-crystals of 1-8 were synthesized and characterized by elemental analysis, FTIR spectroscopy, H-1 NMR and single-crystal X-ray diffraction. The results display the distinct substituent effect on the hydrogen-bonded self-assembly systems. In addition, the luminescent properties of A1-A2 and 1-8 were investigated in the solid state.
引用
收藏
页码：4287 / 4303
页数：17
相关论文
共 73 条
[1]   Expanded capsules with reversibly added spacers [J].
Ajami, D ;
Rebek, J .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2006, 128 (16) :5314-5315
[2]   Longer guests drive the reversible assembly of hyperextended capsules [J].
Ajami, Dariush ;
Rebek, Julius, Jr. .
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2007, 46 (48) :9283-9286
[3]   Coiled molecules in spring loaded devices [J].
Ajami, Dariush ;
Rebek, Julius, Jr. .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2006, 128 (47) :15038-15039
[4]   Solid-state hosts by the template polymerization of columnar liquid crystals: Locked supramolecular architectures around chiral 2-amino alcohols [J].
Amano, Sayaka ;
Ishida, Yasuhiro ;
Saigo, Kazuhiko .
CHEMISTRY-A EUROPEAN JOURNAL, 2007, 13 (18) :5186-5196
[5]   Supramolecular silanol chemistry:: Inclusion complexes of 1,3,5-tris(diisopropylhydroxysilyl)benzene and 4,4′-bis(pyridines) [J].
Beckmann, Jens ;
Jaenicke, Sanna L. .
EUROPEAN JOURNAL OF INORGANIC CHEMISTRY, 2006, (17) :3351-3358
[6]   Cocrystals of 1,3,5-cyclohexanetricarboxylic acid with 4,4′-bipyridine homologues:: Acid•••pyridine hydrogen bonding in neutral and ionic complexes [J].
Bhogala, BR ;
Nangia, A .
CRYSTAL GROWTH & DESIGN, 2003, 3 (04) :547-554
[7]   The 2-aminopyridinium-carboxylate supramolecular heterosynthon: A robust motif for generation of multiple-component crystals [J].
Bis, JA ;
Zaworotko, MJ .
CRYSTAL GROWTH & DESIGN, 2005, 5 (03) :1169-1179
[8]   Intermolecular interactions in nonorganic crystal engineering [J].
Braga, D ;
Grepioni, F .
ACCOUNTS OF CHEMICAL RESEARCH, 2000, 33 (09) :601-608
[9]   Crystal engineering and organometallic architecture [J].
Braga, D ;
Grepioni, F ;
Desiraju, GR .
CHEMICAL REVIEWS, 1998, 98 (04) :1375-1405
[10]   Solid-state preparation of hybrid organometallic-organic macrocyclic adducts with long chain dicarboxylic acids [J].
Braga, Dario ;
Giaffreda, Stefano Luca ;
Grepioni, Fabrizia .
CHEMICAL COMMUNICATIONS, 2006, (37) :3877-3879
12345678