Synthesis of trans-bis(glycinato) copper(II) complex nanorods by room temperature solid-state reaction

被引：11
作者：
Wang, L
Liu, L
Jia, DZ [1 ]
Cao, YL
Xin, XQ
机构：
[1] Xinjiang Univ, Inst Appl Chem, Urumqi 830046, Peoples R China
[2] Nanjing Univ, Inst Coordinat Chem, State Key Lab Coordinat Chem, Nanjing 210093, Peoples R China
来源：
CHINESE SCIENCE BULLETIN | 2005年 / 50卷 / 08期
基金：
中国国家自然科学基金;
关键词：
room temperature solid-state reaction; trans-bis(glycinato) copper; surfactant; nanorods;
D O I：
10.1360/04wb0020
中图分类号：
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号：
07 ; 0710 ; 09 ;
摘要：
Trans-[Cu(glyo)(2)(H2O)] nanoparticles with average diameters about 20-30 mn were prepared by one-step room temperature solid-state reaction. Trans-[Cu(glyo)(2)] nanorods with diameters ranging from 100 to 150 nm and lengths up to several pm were also prepared by one-step room temperature solid-state reaction in the presence of a suitable nonionic surfactant PEG400. The chemical composition and structural features of the products were investigated by elemental analyses, XRD, TG, SEM and TEM, respectively. The mechanisms of formation were also discussed.
引用
收藏
页码：758 / 760
页数：3
相关论文
共 12 条
[1]   Synthesis of gallium nitride nanorods through a carbon nanotube-confined reaction [J].
Han, WQ ;
Fan, SS ;
Li, QQ ;
Hu, YD .
SCIENCE, 1997, 277 (5330) :1287-1289
[2]   Synthesis of CuO nanometer powder by one step solid state reaction at room temperature [J].
Jia, DZ ;
Yu, JQ ;
Xia, X .
CHINESE SCIENCE BULLETIN, 1998, 43 (07) :571-573
[3]  
JIA DZ, 1993, ACTA CHIM SINICA, V51, P358
[4]   Syntheses of perovskite-type composite oxides nanocrystals by solid-state reactions [J].
Li, F ;
Zheng, HG ;
Jia, DZ ;
Xin, XQ ;
Xue, ZL .
MATERIALS LETTERS, 2002, 53 (4-5) :282-286
[5]   A microwave assisted heating method for the preparation of copper sulfide nanorods [J].
Liao, XH ;
Chen, NY ;
Xu, S ;
Yang, SB ;
Zhu, JJ .
JOURNAL OF CRYSTAL GROWTH, 2003, 252 (04) :593-598
[6]   Hydrothermal synthesis of ZnO nanorods in the diameter regime of 50 nm [J].
Liu, B ;
Zeng, HC .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2003, 125 (15) :4430-4431
[7]   Nanotechnology - Carbon-based electronics [J].
McEuen, PL .
NATURE, 1998, 393 (6680) :15-+
[8]   A laser ablation method for the synthesis of crystalline semiconductor nanowires [J].
Morales, AM ;
Lieber, CM .
SCIENCE, 1998, 279 (5348) :208-211
[9]   Nanobelts of semiconducting oxides [J].
Pan, ZW ;
Dai, ZR ;
Wang, ZL .
SCIENCE, 2001, 291 (5510) :1947-1949
[10]   Carbon nanotubes for next-generation electronics devices [J].
Saito, S .
SCIENCE, 1997, 278 (5335) :77-78
12