Synthesis and Crystal Structure of (E)-Ethyl 2-(4-(2,4-dimethoxybenzylideneamino)-5-(3,4,5-trimethoxyphenyl)-4H-1,2,4-triazol-3-ylthio)acetate

被引：0

作者：

You Wen-Wei ^{[1
]}

Zhao Pei-Liang ^{[1
]}

Duan An-Na ^{[1
]}

Wu Shu-Guang ^{[1
]}

机构：

[1] So Med Univ, Dept Chem, Coll Pharmaceut Sci, Guangzhou 510515, Guangdong, Peoples R China

来源：

CHINESE JOURNAL OF STRUCTURAL CHEMISTRY | 2011年 / 30卷 / 04期

关键词：

synthesis; crystal structure; (Z)-methyl 3-methoxy-2-{2-[(4-(E-3-p-tolylacryloyl)phenoxy)methyl]phenyl}acrylate; MANNICH-BASES; ANALOGS; MOIETY; DERIVATIVES; SCHIFF; AGENTS; ACID;

D O I：

暂无

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The crystal structure of the title compound (E)-ethyl 2-(4-(2,4-dimethoxy benzylideneamino)-5-(3,4,5-trimethoxyphenyl)-4H-1,2,4-triazol-3-ylthio)acetate (4, C(24)H(28)N(4)O(7)S, M(r) = 516.17) was synthesized and determined by X-ray single-crystal diffraction. The crystal belongs to the monoclinic system, space group P2(1)/n with a = 13.162(2), b = 8.4506(13), c = 22.602(4) angstrom, beta = 99.888(3)degrees, mu = 0.183 mm(-1), V = 2476.5(7) angstrom(3), Z = 4, D(c) = 1.385 g/cm(3), F(000) = 1088, T = 110(2) K, R = 0.0426 and wR = 0.1216 for 3859 observed reflections with I > 2 sigma(I).

引用

页码：600 / 603

页数：4

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