Determination of sulfonamides in livers using matrix solid-phase dispersion extraction high-performance liquid chromatography

被引：26

作者：

Zhang, Yupu ^{[2
,3
]}

Xu, Xu ^{[2
]}

Qi, Xiao ^{[3
]}

Gao, Wenquan ^{[3
]}

Sun, Shuo ^{[2
]}

Li, Xiaotian ^{[2
]}

Jiang, Chengfei ^{[2
]}

Yu, Aimin ^{[2
]}

Zhang, Hanqi ^{[2
]}

Yu, Yong ^{[1
]}

机构：

[1] Jilin Univ, Coll Instrumentat & Elect Engn, Changchun 130061, Peoples R China

[2] Jilin Univ, Coll Chem, Changchun 130061, Peoples R China

[3] Natl Tobacco Corp China, Jilin Subsidiary, Changchun, Peoples R China

来源：

JOURNAL OF SEPARATION SCIENCE | 2012年 / 35卷 / 01期

关键词：

Fluorescence detection; High-performance liquid chromatography; Liver; Matrix solid-phase dispersion; TANDEM MASS-SPECTROMETRY; ULTRAVIOLET DETECTION; POSTCOLUMN DERIVATIZATION; FLUORESCENCE DETECTION; RESIDUES; TISSUES; ANTIBIOTICS; HONEY; WATER; EGGS;

D O I：

10.1002/jssc.201100600

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The matrix solid-phase dispersion (MSPD) was applied for extracting seven sulfonamides (SAs) in liver samples. The separation and determination were carried out by high-performance liquid chromatography. The analytes were derivated with fluorescamine and detected with fluorescence detector. The types of dispersion adsorbents for MSPD were examined and the highest recovery was obtained when the diatomaceous earth was used as the dispersion adsorbent and the mass ratio of dispersion adsorbent to sample was 3:1. The acetone was used as the elution solvent. Under the optimal conditions, the linear range for determining the SAs in liver samples was 5.0-1000.0 ng/g. The porcine, chicken and cattle liver samples were analyzed and the average recoveries of seven SAs were higher than 84.6%.

引用

页码：45 / 52

页数：8

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