Enhancement by Spark Discharge in LIBS Detection of Copper Particle Contamination in Oil-Immersed Transformer

被引:4
|
作者
Ye, Zhe [1 ]
Ke, Wei [1 ]
Wang, Wanting [2 ]
Yuan, Huan [1 ]
Wang, Xiaonan [1 ]
Wang, Xiaohua [1 ]
Liu, Dingxin [1 ]
Yang, Aijun [1 ]
Rong, Mingzhe [1 ]
机构
[1] Xi An Jiao Tong Univ, State Key Lab Elect Insulat & Power Equipment, Xian 710049, Peoples R China
[2] Hangzhou Elect Power Equipment Mfg Co Ltd, Linan Hengxin Complete Elect Mfg Branch, Hangzhou 311301, Peoples R China
基金
中国博士后科学基金; 中国国家自然科学基金;
关键词
Copper particle; enhancement; laser-induced breakdown spectroscopy (LIBS); spark discharge; INDUCED BREAKDOWN SPECTROSCOPY; LASER-INDUCED PLASMA; ABLATION; METALS;
D O I
10.1109/TDEI.2022.3198757
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
The detection of copper particles in transformer oil based on laser-induced breakdown spectroscopy (LIBS) technology has been preliminarily studied, but its limit of detection (LOD) needs to be further strengthened. Therefore, spark-discharge assistant method was used to solve the problem, and its enhancement mechanism has been studied in the research. The study of the correlation between spark-discharge-assisted LIBS (SD-LIBS) spectral intensity and Cu concentration shows that spark discharge has a significant increase in plasma size and spectral intensity; for Cu atomic lines at 324.75 and 327.39 nm, the determination coefficient R-2 between their internal standard correction intensity and Cu concentration is promoted to 0.996 and 0.997, respectively; spark-discharge assistant method improves the LOD of LIBS from 0.775 to 0.112 mu g/g. Due to the great improvement in detection performance, the application prospect of LIBS as fine particles detection method in transformer oil has become practical.
引用
收藏
页码:2034 / 2041
页数:8
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