The crystal structure of the first ether solvate of hexaphenyldistannane [(Ph3Sn)2•2 THF]

被引：11
|
作者：
Bauer, Jonathan O. [1 ]
机构：
[1] Univ Regensburg, Fak Chem & Pharm, Inst Anorgan Chem, Univ Str 31, D-93053 Regensburg, Germany
来源：
MAIN GROUP METAL CHEMISTRY | 2020年 / 43卷 / 01期
关键词：
crystalline solvates; inclusion compounds; stannanes; tin; weak interactions; X-ray crystallography; MOLECULAR-STRUCTURE; TRIVALENT CARBON; HYDROGEN; ANALOGS; POLYMORPHISM; ANIONS; BONDS; TIN;
D O I：
10.1515/mgmc-2020-0001
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Structural investigations of molecular crystal solvates can provide important information for the targeted crystallization of particular inclusion compounds. Here, the crystal structure of the first ether solvate of hexaphenyldistannane [(Ph3Sn)(2)center dot 2 THF] is reported. Structural features in terms of host-guest interactions and in the context of the previously reported polymorphs and solvates of (Ph3Sn)(2) are discussed.
引用
收藏
页码：1 / 6
页数：6
相关论文
共 50 条
  • [1] Synthesis, spectroscopic characterization and structural studies of organotin monothiocarbonates.: Crystal structures of Ph3Sn[SCO2Me] and Ph3Sn[SCO2(i-Pr)]
    Drake, JE
    Yang, JC
    CANADIAN JOURNAL OF CHEMISTRY-REVUE CANADIENNE DE CHIMIE, 2000, 78 (09): : 1214 - 1221
  • [2] (Me2NH2)[(Ph3Sn)3(MoO4)2], a triorganotin molybdate with layer structure
    Kondracka, Malgorzata
    Merzweiler, Kurt
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2007, 633 (08): : 1131 - 1133
  • [3] Crystal and Molecular Structure of the trans-Hyponitrite Compound Ph3Sn(μ-ONNO)SnPh3
    Mayer, Tobias
    Beck, Wolfgang
    Boettcher, Hans-Christian
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2011, 637 (3-4): : 345 - 347
  • [4] [(Ph3Sn)3VO4]•CH3CN and [(Ph3Sn)3VO4]•2 DMF, triphenyltin vanadates with novel chain structures
    Herntrich, Tobias
    Merzweiler, Kurt
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2006, 632 (14): : 2341 - 2344
  • [5] The crystal structures of (NBu4)[(Ph3Sn)3(MoO4)2] and (NBu4)[(Ph3Sn)3(MoO4)2]•CH3CN:: Organotin molybdates with novel 3D networks
    Rosenland, F
    Kondracka, M
    Merzweiler, K
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2003, 629 (14): : 2573 - 2576
  • [6] 4,5-Bis[(triorganotin)thiolato]-1,3-dithiole-2-thione, (R3Sn)2(dmit), 4,5-bis [(triorganotin)thiolato]-1,3-dithiole-2-one, (R3Sn)2(dmio), compounds:: Crystal structures of (cyclohexyl3Sn)2(dmio), (Ph3Sn)2(dmit) and (Ph3Sn)2(dmio)
    Bordinhao, J
    Comerlato, NM
    Ferreira, GB
    Howie, RA
    da Silva, CXA
    Wardell, JL
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 2006, 691 (08) : 1598 - 1605
  • [7] Crystal Structures and Spectral Studies of [Ph3Sn(O2AsMe2)] [Bu2ClSn(O2AsMe2)] and [PhClSn(O2AsMe2)(μ-OMe)]2
    Shihada, Abdel-Fattah
    Weller, Frank
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2008, 634 (02): : 339 - 344
  • [8] Synthesis and Properties of Ph3Sn substituted Tellurates - The Crystal Structures of trans-[(Ph3SnO)4Te(OH)2] and trans-[(Ph3SnO)2Te(OMe)4]
    Herntrich, Tobias
    Merzweiler, Kurt
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2010, 636 (05): : 803 - 807
  • [9] SYNTHESIS AND CRYSTAL-STRUCTURES OF THE CYCLOSILOXYTIN(IV) COMPLEXES [CL2SN(O(SIPH(2)O)(2))(2)]-MU-(LI(THF)(2))(2)] AND [THF2SN((OSIPH(2))(3)O)(2)]CENTER-DOT-TOLUENE
    ABRAHAMS, I
    MOTEVALLI, M
    SHAH, SAA
    SULLIVAN, AC
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1995, 492 (01) : 99 - 104
  • [10] Synthesis and Reactivity of Donor-Stabilized Bis(pentafluoroethyl)stannylene [Sn(C2F5)2(D)n] (D=THF, DMAP, PMe3, [Sn(C2F5)3]-)
    Kloesener, Johannes
    Wiesemann, Markus
    Niemann, Mark
    Neumann, Beate
    Stammler, Hans-Georg
    Hoge, Berthold
    CHEMISTRY-A EUROPEAN JOURNAL, 2018, 24 (17) : 4412 - 4422
12345