A microwave assisted synthesis of 3,4-dihydropyrimidin-2(1H)-ones and thiones using NiFe2O4 ferrite as an. effective, and reusable catalyst

被引:0
作者
Ladole, C. A. [1 ]
Salunkhe, N. G. [1 ]
Aswar, A. S. [1 ]
机构
[1] St Gadge Baba Amravati Univ, Dept Chem, Amravati 444602, Maharashtra, India
关键词
Biginelli reaction; NiFe2O4; ferrite; 3,4-dihydropyrimidine-2-(1H)-ones/thiones; microwave; ONE-POT SYNTHESIS; HYDROGEN-TRANSFER REDUCTION; CARBONYL-COMPOUNDS; RECYCLABLE CATALYSTS; NICKEL NANOPARTICLES; SOLVENT-FREE; EFFICIENT; CHEMISTRY;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A microwave assisted one pot synthesis of 3,4-dihydropyrimidin-2(1H)-one/thione derivatives in solvent free conditions by using reusable NiFe2O4 ferrite as an inexpensive and efficient catalyst is described. The catalyst NiFe2O4 ferrite prepared by co-precipitation method followed by calcination, and characterized by XRD, FT-IR, TG-DTA and SEM analysis for evaluating its structure and morphological analysis. Synthesis of 3,4-dihydropyrimidin-2(1H)-one/thione derivatives over NiFe2O4 offers several advantages over conventional method such as simple reaction conditions, high product yields, short reaction time and environmentally benign reaction conditions.
引用
收藏
页码:337 / 344
页数:8
相关论文
共 34 条
[1]   Synthesis and characterization of nickel ferrite nanoparticles by chemical method [J].
Aliahmad, M. ;
Noori, M. .
INDIAN JOURNAL OF PHYSICS, 2013, 87 (05) :431-434
[2]   Hydrogen-transfer reductive amination of aldehydes catalysed by nickel nanoparticles [J].
Alonso, Francisco ;
Riente, Paola ;
Yus, Miguel .
SYNLETT, 2008, (09) :1289-1292
[3]   Hydrogen-transfer reduction of carbonyl compounds promoted by nickel nanoparticles [J].
Alonso, Francisco ;
Riente, Paola ;
Yus, Miguel .
TETRAHEDRON, 2008, 64 (08) :1847-1852
[4]   Hydrogen-transfer reduction of carbonyl compounds catalysed by nickel nanoparticles [J].
Alonso, Francisco ;
Riente, Paola ;
Yus, Miguel .
TETRAHEDRON LETTERS, 2008, 49 (12) :1939-1942
[5]   The tethered Biginelli condensation in natural product synthesis [J].
Aron, ZD ;
Overman, LE .
CHEMICAL COMMUNICATIONS, 2004, (03) :253-265
[6]   An efficient microwave-assisted Suzuki cross-coupling reaction of imidazo[1,2-a]pyridines in aqueous medium [J].
Crozet, Maxime D. ;
Castera-Ducros, Caroline ;
Vanelle, Patrice .
TETRAHEDRON LETTERS, 2006, 47 (39) :7061-7065
[7]   Solid- and solution-phase synthesis of bioactive dihydropyrimidines [J].
Dallinger, D ;
Stadler, A ;
Kappe, CO .
PURE AND APPLIED CHEMISTRY, 2004, 76 (05) :1017-1024
[8]   Microwave-assisted synthesis in water as solvent [J].
Dallinger, Doris ;
Kappe, C. Oliver .
CHEMICAL REVIEWS, 2007, 107 (06) :2563-2591
[9]   The first catalytic, asymmetric α-additions of isocyanides.: Lewis-base-catalyzed, enantioselective Passerini-type reactions [J].
Denmark, SE ;
Fan, Y .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2003, 125 (26) :7825-7827
[10]   Clay entrapped nickel nanoparticles as efficient and recyclable catalysts for hydrogenation of olefins [J].
Dhakshinamoorthy, Amarajothi ;
Pitchumani, Kasi .
TETRAHEDRON LETTERS, 2008, 49 (11) :1818-1823