5′-Methylsulfanyl-4′-oxo-7′-phenyl-3′,4′-dihydro-1′H-spiro[cyclohexane-1,2′-quinazoline]-8′-carbonitrile dimethylformamide monosolvate

被引：5

作者：

Liu, Xuan ^{[1
]}

Shi, Daxin ^{[1
]}

Tang, Jianhong ^{[1
,2
]}

Yang, Deli ^{[1
]}

Li, Jiarong ^{[1
]}

机构：

[1] Beijing Inst Technol, Sch Chem Engn & Environm, Beijing 100081, Peoples R China

[2] Huaqiao Univ, Coll Chem Engn, Xiamen 362021, Fujian, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷

关键词：

data-to-parameter ratio = 19.8; mean σ(CC) = 0.002 Å; R factor = 0.047; single-crystal X-ray study; T = 153 K; wR factor = 0.117;

D O I：

10.1107/S1600536811026948

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C21H21N3OS center dot C3H7NO, the carbonitrile molecule is built up of two fused six-membered rings and one six-membered ring linked through a spiro C atom. The 1,3-diaza ring adopts an envelope conformation and the cyclohexane ring adopts a chair conformation. The dihedral angle between the aromatic rings is 46.7 ( 3)degrees. In the crystal, the components are linked by N-H center dot center dot center dot O hydrogen bonds.

引用

页码：O2016 / U334

页数：11

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