Structure, microhardness and thermal conducting properties of the high-pressure high-temperature-treated Al-Ti-N materials

被引:2
作者
Kudyakova, V. S. [1 ]
Chukin, A. V. [1 ]
Dorokhin, M. V. [2 ]
Kuznetsov, Yu. M. [2 ]
Shishkin, R. A. [1 ]
Beketov, A. R. [1 ]
机构
[1] Ural Fed Univ, Ekaterinburg 620002, Russia
[2] Lobachevsky State Univ Nizhni Novgorod, Phys Tech Res Inst, Nizhnii Novgorod, Russia
来源
APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING | 2019年 / 125卷 / 02期
关键词
ALUMINUM NITRIDE;
D O I
10.1007/s00339-019-2415-1
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The w-AlN rs-AlN polymorphic transition in Ti-Al-N system with low TiN content (3mol%) was observed. The experimental data show that this transition is possible under 12GPa pressure at 1773K. The formation of rs-AlN phase in the resulting composite materials was confirmed by XRD. The obtained materials have intermediate physical and mechanical properties as compared to the undoped w-AlN and TixAl1-xN solid solution. They are found to have high Vickers hardness (31GPa at a load of 50g)which is twice as hard as w-AlN. The thermal conductivity of the rs-AlN-containing Al-Ti-N materials was measured for the first time using the frequency separation (3) method and gave high thermal conductivity coefficients up to 100W/mxK.
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页数:9
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