Determination of Trans-resveratrol in Wines, Spirits, and Grape Juices Using Solid-Phase Micro Extraction Coupled to Liquid Chromatography with UV Diode-Array Detection

被引：25

作者：

Aresta, Antonella ^{[1
]}

Cotugno, Pietro ^{[2
]}

Massari, Federica ^{[1
]}

Zambonin, Carlo ^{[1
]}

机构：

[1] Univ Bari Aldo Moro, Dept Chem, Via Orabona 4, I-70125 Bari, Italy

[2] CONISMA, Piazzale Flaminio 9, I-00196 Rome, Italy

来源：

FOOD ANALYTICAL METHODS | 2018年 / 11卷 / 02期

关键词：

Trans-resveratrol; SPME; LC/UV-DAD; Wines; Spirits; Grape juices; MASS-SPECTROMETRY; PHENOLIC-COMPOUNDS; PROSTATE-CANCER; CIS-RESVERATROL; MICROEXTRACTION; POLYPHENOLS; STILBENES; PICEID; SYSTEM;

D O I：

10.1007/s12161-017-1013-0

中图分类号：

TS2 [食品工业];

学科分类号：

0832 ;

摘要：

Solid phase microextraction (polyacrylate fiber), coupled to liquid chromatography with UV diode-array detection, has been optimized for the determination of trans-resveratrol in wines, spirits, and grape juices. The main aspects influencing fiber adsorption (fiber coating, extraction time, ethanol content, salt addition) and desorption (desorption and injection time, desorption solvent mixture composition, carryover) of the analyte have been investigated. The method permitted a fast and simple determination of free trans-resveratrol in commercial samples. It was found in all the analyzed samples at concentration levels ranging from 0.007 to 4.486 mu g mL(-1). Total trans-resveratrol concentrations were also evaluated after enzymatic deconjugation of piceid.

引用

页码：426 / 431

页数：6

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