Plant protection product residues in red grapes and Teran PTP wine

被引:6
作者
Cesnik, Helena Basa [1 ]
Bolta, Spela Velikonja [1 ]
Lisjak, Klemen [2 ]
机构
[1] Agr Inst Slovenia, Cent Labs, Ljubljana, Slovenia
[2] Agr Inst Slovenia, Dept Fruit Growing Viticulture & Oenol, Ljubljana, Slovenia
来源
FOOD ADDITIVES & CONTAMINANTS PART B-SURVEILLANCE | 2015年 / 8卷 / 02期
关键词
Kras (Karst); grapes; wine; Teran PTP; plant protection product residues; GC; MS; LC; RAPID-DETERMINATION; MULTIRESIDUE METHOD; MASS-SPECTROMETRY; PESTICIDES; LIQUID; FATE; TRIFLOXYSTROBIN; CHLORPYRIFOS; INSECTICIDES; PENCONAZOLE;
D O I
10.1080/19393210.2014.1002816
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
Between 2011 and 2013, a total of 73 grape and 82 wine samples from winegrowing district Kras (Karst) were analysed for plant protection product (PPP) residues. The samples were analysed for the presence of 215 different active compounds using two multiresidual analytical methods: gas chromatography coupled with mass spectrometry and liquid chromatography coupled with tandem mass spectrometry. Residues were found in 91.8% of all grape samples and in 67.1% of all wine samples. In all grape samples, residues were below maximum residue levels (MRLs) and 58.9% of all grape samples contained active substances at a level of less then 10% of the MRL. Nearly 33% of all Teran PTP wines did not contain PPP residues at all. Residues diminish during processing of grapes to wine, so their content in wine was low. Therefore, it could be concluded that grapes and wine in the winegrowing district Kras are safe for consumers.
引用
收藏
页码:113 / 122
页数:10
相关论文
共 29 条
[1]   Validation and global uncertainty of a liquid chromatographic with diode array detection method for the screening of azoxystrobin, kresoxim-methyl, trifloxystrobin, famoxadone, pyraclostrobin and fenamidone in grapes and wine [J].
Abreu, Susana de Melo ;
Caboni, Pierluigi ;
Cabras, Paolo ;
Garau, Vincenzo Luigi ;
Alves, Arminda .
ANALYTICA CHIMICA ACTA, 2006, 573 :291-297
[2]   Fate of Iprovalicarb, Indoxacarb, and Boscalid Residues in Grapes and Wine by GC-ITMS Analysis [J].
Angioni, Alberto ;
Dedola, Fabrizio ;
Garau, Vincenzo Luigi ;
Schirra, Mario ;
Caboni, Pierluigi .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2011, 59 (12) :6806-6812
[3]  
[Anonymous], 1994, Accuracy (trueness and precision) of measurement methods and results - Part 1: General principies and defmitions
[4]  
[Anonymous], 2014, IMEP37 DG JOINT RES
[5]  
BIPEA, 2012, 051319 BIPEA
[6]  
BIPEA (Bureau Interprofessionnel d'Etudes Analytiques), 2022, Interlaboratory Comparisons Report
[7]   Pesticide residues in grapes, wine, and their processing products [J].
Cabras, P ;
Angioni, A .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2000, 48 (04) :967-973
[8]   Fate of some new fungicides (cyprodinil, fludioxonil, pyrimethanil, and tebuconazole) from vine to wine [J].
Cabras, P ;
Angioni, A ;
Garau, VL ;
Melis, M ;
Pirisi, FM ;
Minelli, EV ;
Cabitza, F ;
Cubeddu, M .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1997, 45 (07) :2708-2710
[9]   Pesticide residues in grapes from vineyards included in integrated pest management in Slovenia [J].
Cesnik, H. Basa ;
Gregorcic, A. ;
Cus, F. .
FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT, 2008, 25 (04) :438-443
[10]   Fast low-pressure gas chromatography-mass spectrometry method for the determination of multiple pesticides in grapes, musts and wines [J].
Cunha, S. C. ;
Fernandes, J. O. ;
Alves, A. ;
Oliveira, M. B. P. P. .
JOURNAL OF CHROMATOGRAPHY A, 2009, 1216 (01) :119-126