Mechanism of the α-ε phase transformation in iron

被引:61
作者
Dewaele, A. [1 ]
Denoual, C. [1 ]
Anzellini, S. [1 ]
Occelli, F. [1 ]
Mezouar, M. [2 ]
Cordier, P. [3 ]
Merkel, S. [3 ]
Veron, M. [4 ]
Rausch, E. [4 ]
机构
[1] Commissariat Energie Atom, Direct Applicat Militaires, F-91297 Arpajon, France
[2] European Synchrotron Radiat Facil, F-38043 Grenoble, France
[3] Univ Lille 1, UMR CNRS 8207, Unite Materiaux & Transformat, F-59655 Villeneuve Dascq, France
[4] Grenoble INP CNRS UJF, Lab SIMaP, F-38402 St Martin Dheres, France
来源
PHYSICAL REVIEW B | 2015年 / 91卷 / 17期
关键词
HIGH-PRESSURE; MARTENSITIC-TRANSFORMATION; TRANSITION; ORIENTATION; CALIBRATION; HELIUM; GAUGE; GPA;
D O I
10.1103/PhysRevB.91.174105
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The alpha-Fe <-> is an element of-Fe pressure-induced transformation under pure hydrostatic static compression has been characterized with in situ x-ray diffraction using alpha-Fe single crystals as starting samples. The forward transition starts at 14.9 GPa, and the reverse at 12 GPa, with a width of alpha-is an element of coexistence domain of the order of 2 GPa. The elastic stress in the sample increases in this domain, and partially relaxes after completion of the transformation. Orientation relations between parent alpha-Fe and child is an element of-Fe have been determined, which definitely validates the Burgers path for the direct transition. On the reverse transition, an unexpected variant selection is observed. X-ray diffraction data, complemented with ex situ microstructural observations, suggest that this selection is caused by defects and stresses accumulated during the direct transition.
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页数:8
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