Preparation and characterization of porous Al2O3 based on nano-Al2O3 powders and PLA template by microwave sintering

被引：0
作者：
He, Zhenhua [1 ]
Zhu, Shifei [1 ]
Liu, Canhui [1 ]
机构：
[1] Wuhan Univ Technol, Sch Informat Engn, Wuhan 430070, Peoples R China
来源：
PROCESSING AND APPLICATION OF CERAMICS | 2020年 / 14卷 / 02期
基金：
中国国家自然科学基金;
关键词：
porous Al2O3; 3D printing; microwave sintering; advanced manufacturing; ALUMINA; CERAMICS; FABRICATION;
D O I：
10.2298/PAC2002128H
中图分类号：
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
Macroporous and mesoporous Al2O3 body was prepared using mesh screening shaped polylactic acid (PLA) template. The mesh screening shaped PLA template was made from 3D cylindrical model by adjusting the PLA filling rate at 30 vol. %. After 3D printing, the PLA template was filled with Al2O3 nano powders and microwave sintered at 1673 K for 20 min. During the sintering, the PLA template was decomposed and left large pores which could promote sintering of Al2O3. The Al2O3 sintered body showed macroporous structure with the pore size of 100 to 300 nm and also mesoporosity with local single crystal structure. The average pore diameter of mesoporous structures in the Al2O3 sintered body was about 7.6 nm. The Vickers hardness of the porous Al2O3 is 1.254 +/- 0.039 GPa. The obtained results confirmed that 3D-printed PLA template assisted microwave sintering is a promising technical processing for the fabrication of macroporous and mesoporous Al2O3 with local single crystal structure.
引用
收藏
页码：128 / 133
页数：6
相关论文
共 50 条
[41]   Effect of Precursors on the Preparation and Texture of Mesoporous γ-Al2O3 Powders [J].
Morozova, L. V. ;
Khamova, T. V. ;
Polyakova, I. G. .
INORGANIC MATERIALS, 2020, 56 (04) :353-359
[42]   Ti-based nanocoatings on Al2O3 powders [J].
Villegas, M. ;
Sierra, T. ;
Caballero, A. C. ;
Fernandez, J. F. .
CERAMICS INTERNATIONAL, 2007, 33 (05) :875-878
[43]   Production of α-Al2O3-3YSZ Porous Ceramics with α(γ)-Al2O3 Additive [J].
Komolikov, Yu. I. ;
Ermakova, L. V. ;
Shishkin, R. A. ;
Skachkov, V. M. ;
Zhuravlev, V. D. .
GLASS AND CERAMICS, 2025, 81 (9-10) :373-379
[44]   Preparation and properties of an Al2O3/Ti(C,N) micro-nano-composite ceramic tool material by microwave sintering [J].
Yin, Zengbin ;
Yuan, Juntang ;
Wang, Zhenhua ;
Hu, Hanpeng ;
Cheng, Yu ;
Hu, Xiaoqiu .
CERAMICS INTERNATIONAL, 2016, 42 (03) :4099-4106
[45]   Preparation of spherical α-Al2O3 nanoparticles by microwave hydrothermal synthesis and addition of nano-Al seeds [J].
Wang, Zhiyuan ;
Mai, Zenghui ;
Wu, Yixiao ;
Wang, Ying ;
Cao, Zhenzhen ;
Li, Mingliang ;
Fan, Bingbing ;
Shao, Gang ;
Wang, Hailong ;
Xu, Hongliang ;
Zhang, Rui ;
Lu, Hongxia .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2022, 105 (09) :5585-5597
[46]   Synthesis and characterization of monodisperse porous α-Al2O3 nanoparticles [J].
Su, Xinghua ;
Chen, Shuanfa ;
Zhou, Zhenjun .
APPLIED SURFACE SCIENCE, 2012, 258 (15) :5712-5715
[47]   The Effect of nano-Al2O3 on Sintering Behavior and Mechanical Property of ZrO2 Ceramics [J].
Yi, Zhongzhou ;
Sun, Hongyan ;
Wang, Bo ;
Zhai, Fengrui ;
Xie, Zhipeng .
HIGH-PERFORMANCE CERAMICS VIII, 2014, 602-603 :327-330
[48]   Experimental and Theoretical Study of Porous Al2O3 [J].
Parhizgar, Sara Sadat ;
Taheriniya, Shabnam ;
Beheshtian, Javad .
TRANSACTIONS OF THE INDIAN INSTITUTE OF METALS, 2021, 74 (02) :381-386
[49]   Preparation, characterization, and in vitro release of ibuprofen from Al2O3/PLA/PMMA composites [J].
Vallet-Regí, M ;
Granado, S ;
Arcos, D ;
Gordo, M ;
Cabañas, MV ;
Ragel, CV ;
Salinas, AJ ;
Doadrio, AL ;
San Román, J .
JOURNAL OF BIOMEDICAL MATERIALS RESEARCH, 1998, 39 (03) :423-428
[50]   3D Printing of Porous Al2O3 and SiC ceramics [J].
Polzin, C. ;
Guenther, D. ;
Seitz, H. .
JOURNAL OF CERAMIC SCIENCE AND TECHNOLOGY, 2015, 6 (02) :141-145
12345