Synthesis and characterization of ZnO nanoparticles prepared in gelatin media

被引:175
作者
Zak, A. Khorsand [1 ]
Abd Majid, W. H. [1 ]
Darroudi, Majid [2 ]
Yousefi, Ramin [3 ]
机构
[1] Univ Malaya, Low Dimens Mat Res Ctr, Dept Phys, Fac Sci, Kuala Lumpur 50603, Malaysia
[2] Ferdowsi Univ Mashhad, Dept Chem, Fac Sci, Mashhad 917751436, Iran
[3] Islamic Azad Univ, Dept Phys, Masjed Soliman Branch, Masjed Soliman, Iran
关键词
Nanomaterials; Powder technology; Semiconductors; Sol-gel preparation; HYDROTHERMAL SYNTHESIS;
D O I
10.1016/j.matlet.2010.09.029
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Zinc oxide nanoparticles (ZnO NPs) were synthesized via the sol-gel method in gelatin media Long-chain gelatin compounds were utilized to terminate the growth of ZnO-NPs and to stabilize them The ZnO-NPs were characterized by a number of techniques such as X-ray diffraction analysis (XRD) Fourier transform infrared spectroscopy (FTIR) and high-magnification transmission electron microscopy (TEM) The ZnO-NPs calcined at different temperatures exhibited a hexagonal (wurtzite) structure with sizes from 30 to 60 nm The influence of the calcination temperature on the morphology of ZnO-NPs was also investigated The results showed that gelatin is an interesting material that can be used as a stabilizer in the sol-gel technique for preparing small ZnO-NPs (C) 2010 Elsevier B V All rights reserved
引用
收藏
页码:70 / 73
页数:4
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