Dual ambient plasma source ionization mass spectrometry for the rapid detection of trace sterols in urban water Rapid detection of trace sterols in urban water

被引:12
作者
Zhao, Gaosheng [1 ]
Chu, Fengjian [2 ]
Zhou, Jianguang [1 ,3 ]
机构
[1] Zhejiang Univ, Res Ctr Analyt Instrumentat, Inst Cyber Syst & Control, State Key Lab Ind Control Technol, Hangzhou 310027, Peoples R China
[2] Zhejiang Univ, Coll Informat Sci & Elect Engn, Hangzhou, Peoples R China
[3] Zhejiang Univ, Dept Chem, Hangzhou, Zhejiang, Peoples R China
来源
JOURNAL OF MASS SPECTROMETRY | 2022年 / 57卷 / 02期
关键词
dual ambient plasma source tandem mass spectrometry; high sensitivity; rapid detection technology; sterol detection; urban water; ELECTROSPRAY-IONIZATION; ATMOSPHERIC-PRESSURE; SENSITIVE ANALYSIS; ION-SOURCE; ESTROGENS; PROFILES; SAMPLES; TORCH;
D O I
10.1002/jms.4809
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
A direct analytical method based on dual ambient plasma ion source tandem mass spectrometry was used for the simultaneous determination of four sterols in the environment. This technology has very high sensitivity and the method detects the four sterols in methanol-water (1:3) solutions with limits of detection (LOD) and limits of quantification (LOQ) ranging from 1.2 ng/L to 6.9 ng/L and 7.6 ng/L to 10.0 ng/L, respectively. The method was also used to test water quality at three locations within the city and successfully detected all four sterols at very low concentrations. The dual plasma source tandem mass spectrometry technique is extremely simple, rapid, sensitive and highly efficient compared to other traditional methods, providing a useful screening tool for sterols in water.
引用
收藏
页数:7
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