Microwave Assisted Synthesis of Chitosan Nanoparticles

被引：11
|
作者：
Kocak, Nuriye [2 ]
Sahin, Mustafa [1 ]
Akin, Ilker [1 ]
Kus, Mahmut [3 ]
Yilmaz, Mustafa [1 ]
机构：
[1] Selcuk Univ, Fac Sci, Dept Chem, TR-42075 Konya, Turkey
[2] Selcuk Univ, Fac Educ, Dept Sci Educ, TR-42075 Konya, Turkey
[3] Selcuk Univ, Fac Architectural Engn, Dept Chem Engn, TR-42075 Konya, Turkey
来源：
JOURNAL OF MACROMOLECULAR SCIENCE PART A-PURE AND APPLIED CHEMISTRY | 2011年 / 48卷 / 10期
关键词：
Chitosan nanoparticle; tripolyphosphate; microwave irradiation; ionotropic gelation; DELIVERY; ADSORPTION;
D O I：
10.1080/10601325.2011.603613
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
Chitosan nanoparticles (CHN) were prepared based on ionotropic gelation between low moleculer weight chitosan and sodium tripolyphosphate (TPP) under microwave irradiation. Particle size, zeta potential, and FT-IR techniques were used for characterization of CHN. The influence of reaction time on the nanoparticle size distribution was investigated, and the results showed that the microwave irradiation method evidently decreases the reaction times and particle size over the conventional method. It was determined by the results of the zeta potential measurements that synthesized CHN under microwave irradiation clearly exhibits more homogeneous and stable dispersion.
引用
收藏
页码：776 / 779
页数：4
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