Tandem AN-AN reactions in the synthesis of tetrahydrothiazolo[4,5-e][1,2,4]triazines

被引：2
|
作者：
Mochulskaya, Nataliya N. [1 ,2 ]
Slepukhin, Pavel A. [1 ,2 ]
Charushin, Valery N. [1 ,2 ]
Kodess, Mikhail I. [1 ,2 ]
机构：
[1] Ural Fed Univ, Dept Chem, Ekaterinburg 620002, Russia
[2] Russian Acad Sci, Ural Branch, I Ya Postovsky Inst Organ Synth, Ekaterinburg 620041, Russia
来源：
MENDELEEV COMMUNICATIONS | 2016年 / 26卷 / 05期
基金：
俄罗斯科学基金会;
关键词：
1,2,4-TRIAZINES; CHEMISTRY;
D O I：
10.1016/j.mencom.2016.09.002
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Reaction of 3-aryl-1,2,4-triazines with S,N-dinucleophilic N-(het)arylthioureas in acetic anhydride at room temperature affords the cyclization products, tetrahydrothiazolo[4,5-e][1,2,4]triazines in good yields. The structure of the heterocyclic system thus formed was confirmed by X-ray diffraction analysis.
引用
收藏
页码：375 / 377
页数：3
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