Nearly zero thermal expansion of β-spodumene glass ceramics prepared by sol-gel and hot pressing method

被引:23
作者
Xia, Long [1 ]
Wang, Xinyu [1 ]
Wen, Guangwu [1 ]
Zhong, Bo [1 ]
Song, Liang [1 ]
机构
[1] Harbin Inst Technol, Sch Mat Sci & Engn, Weihai 264209, Peoples R China
基金
中国国家自然科学基金;
关键词
Sol-gel processes; Mechanical properties; Thermal expansion; RESIDUAL-STRESSES; TIO2; ADDITION; CRYSTALLIZATION; MICROCRACKING; PRECURSOR;
D O I
10.1016/j.ceramint.2012.03.004
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
beta-Spodumene glass-ceramics were fabricated by sol-gel process followed by hot pressing technique. The microstructure, mechanical properties and thermal expansion behavior of the glass-ceramics were investigated. The glass ceramics hot pressed at 1200 and 1300 degrees C have relative good mechanical properties and nearly zero coefficient of thermal expansion (CTE). CTE of the specimen sintered at 1200 degrees C ranges from -0.03 x 10(-7) K-1 to -0.97 x 10(-7) K-1. The thermal expansion behavior characteristics are found to be strongly influenced by crystalline phases, crystallinity and microstructure in the specimens, which depend on the sintering temperatures. (C) 2012 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
引用
收藏
页码:5315 / 5318
页数:4
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