High-yield microwave synthesis of layered Y2(OH)5NO3.xH2O materials

被引：32
作者：
Yapryntsev, A. D. [1 ,2 ]
Baranchikov, A. E. [2 ]
Skogareva, L. S. [2 ]
Goldt, A. E. [2 ]
Stolyarov, I. P. [2 ]
Ivanova, O. S. [2 ]
Kozik, V. V. [3 ]
Ivanov, V. K. [2 ,3 ]
机构：
[1] Moscow MV Lomonosov State Univ, Moscow 119991, Russia
[2] Russian Acad Sci, NS Kurnakov Gen & Inorgan Chem Inst, Moscow 119991, Russia
[3] Natl Res Tomsk State Univ, Tomsk 634050, Russia
来源：
CRYSTENGCOMM | 2015年 / 17卷 / 13期
关键词：
RARE-EARTH HYDROXIDES; ANION-EXCHANGE MATERIALS; TARGETED DRUG-DELIVERY; GADOLINIUM HYDROXIDE; PHOTOLUMINESCENCE PROPERTIES; CRYSTAL-STRUCTURE; NANOSHEETS; INTERCALATION; LN; NANOPARTICLES;
D O I：
10.1039/c4ce02303j
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A novel, facile, and versatile microwave-assisted method of high-yield synthesis of layered rare earth hydroxo compounds (LRHs) is proposed. Layered yttrium hydroxonitrates synthesized by the microwave-assisted technique crystallize in the form of thin hexagonal plates aggregated into spheroidal particles. Depending on the conditions of microwave-assisted hydrothermal synthesis, the formation of several phases differing in interplanar spacing along the [001] direction is possible. The materials obtained are shown to possess good anion-exchange properties. This work provides a route to large-scale synthesis of LRH-based advanced materials.
引用
收藏
页码：2667 / 2674
页数：8
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