Formation of helium induced nanostructure 'fuzz' on various tungsten grades

被引:339
作者
Baldwin, M. J. [1 ]
Doerner, R. P.
机构
[1] Univ Calif San Diego, Energy Res Ctr, La Jolla, CA 92093 USA
基金
美国能源部;
关键词
LOW-ENERGY; PLASMA IRRADIATION; BLISTER FORMATION; SURFACE; RETENTION; CRYSTALS; METALS; ATOMS;
D O I
10.1016/j.jnucmat.2010.06.034
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The response of a variety of W material grades to nanostructure 'fuzz' formation is explored. W targets are exposed to He or D(2)-0.2He plasmas in PISCES-B at 900-1320 K to below sputter threshold He(+) ions of energy 25-60 eV for up to 2.2 x 10(4) s. SEM and XPS reveal nanoscopic reorganization of the W surface to a layer of 'fuzz' of porosity similar to 90% as determined by a 'fuzz' removal/weight loss method. The variability of 'fuzz' growth is examined at 1120 K for 1 h durations: SR, SC and doped W grades - La(2)O(3) (1% wt.), Re (5% and 10% wt.), and TiC (1.5% wt.) developed 2-3 mu m thick 'fuzz' layers, while a VPS grade developed a layer 4 mu m thick. An RC grade revealed additional 'fuzz' at deep (>100 mu m) grain boundaries. However, heat treatment up to 1900 K produced reintegration of 'fuzz' with the bulk and He release at similar to 1000 K and similar to 1400-1800 K due to depopulation from vacancy complexes. (C) 2010 Elsevier B.V. All rights reserved.
引用
收藏
页码:165 / 173
页数:9
相关论文
共 31 条
[1]   DIFFUSIVITY OF HE-3 ATOMS IN PERFECT TUNGSTEN CRYSTALS [J].
AMANO, J ;
SEIDMAN, DN .
JOURNAL OF APPLIED PHYSICS, 1984, 56 (04) :983-992
[2]   Helium induced nanoscopic morphology on tungsten under fusion relevant plasma conditions [J].
Baldwin, M. J. ;
Doerner, R. P. .
NUCLEAR FUSION, 2008, 48 (03)
[3]   The effects of high fluence mixed-species (deuterium, helium, beryllium) plasma interactions with tungsten [J].
Baldwin, M. J. ;
Doerner, R. P. ;
Nishijima, D. ;
Tokunaga, K. ;
Ueda, Y. .
JOURNAL OF NUCLEAR MATERIALS, 2009, 390-91 :886-890
[4]   SURFACE SELF-DIFFUSION OF TUNGSTEN [J].
BOWDEN, FP ;
SINGER, KE .
NATURE, 1969, 222 (5197) :977-&
[5]   Plasma-surface interaction issues of an all-metal ITER [J].
Brooks, J. N. ;
Allain, P. ;
Doerner, R. P. ;
Hassanein, A. ;
Nygren, R. ;
Rognlien, T. D. ;
Whyte, D. G. .
NUCLEAR FUSION, 2009, 49 (03)
[6]   Codeposition of deuterium with ITER materials [J].
Doerner, R. P. ;
Baldwin, M. J. ;
De Temmerman, G. ;
Hanna, J. ;
Nishijima, D. ;
Roth, J. ;
Schmid, K. ;
Tynan, G. R. ;
Umstadter, K. .
NUCLEAR FUSION, 2009, 49 (03)
[7]  
ECKSTEIN W, 1998, 917 IPP
[8]   Formation process of tungsten nanostructure by the exposure to helium plasma under fusion relevant plasma conditions [J].
Kajita, Shin ;
Sakaguchi, Wataru ;
Ohno, Noriyasu ;
Yoshida, Naoaki ;
Saeki, Tsubasa .
NUCLEAR FUSION, 2009, 49 (09)
[9]   HIGH-TEMPERATURE RECOVERY OF TUNGSTEN AFTER NEUTRON IRRADIATION [J].
KEYS, LK ;
SMITH, JP ;
MOTEFF, J .
PHYSICAL REVIEW, 1968, 176 (03) :851-&
[10]   A STUDY OF BUBBLE NUCLEATION IN TUNGSTEN USING THERMAL-DESORPTION SPECTROMETRY - CLUSTERS OF 2 TO 100 HELIUM-ATOMS [J].
KORNELSEN, EV ;
VANGORKUM, AA .
JOURNAL OF NUCLEAR MATERIALS, 1980, 92 (01) :79-88