Alkoxy-derived ferroelectric PZT films: The effect of lead acetate dehydration techniques and lead content in the electrochemically prepared solutions on the properties of the films

被引:16
作者
Yanovskaya, MI
Obvintseva, IE
Solovyova, LI
Kovsman, EP
Vorotilov, KA
Vasilyev, VA
机构
[1] LY Karpov Phys Chem Res Inst, Moscow 103064, Russia
[2] NIPIM, Tula 300600, Russia
[3] Moscow Inst Radio Engn Elect & Automat, Moscow 117454, Russia
关键词
PZT films; sol-gel techniques; methoxyethanol;
D O I
10.1080/10584589808012704
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
Different ways of dehydration of lead acetate trihydrate for its application in sol-gel techniques are discussed. Reaction of Pb(CH3COO)(2) . 3H(2)O with acetic acid anhydride proved to be the most efficient way of its dehydration. Characteristics of the solutions of lead acetate in methoxyethanol dehydrated by different methods are presented. Solutions for preparation of PZT films are prepared using electrochemical dissolution of titanium and zirconium in methoxyethanol. Physico-chemical properties of these solutions alongside with structural and electrical characteristics of the PZT films obtained from these solutions are presented. The effect of lead content in solutions on the properties of the films obtained is discussed.
引用
收藏
页码:193 / 209
页数:17
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